| 独活寄生颗粒的质量标准研究 |
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| 引用本文： | 赵小勤,蒲旭峰.独活寄生颗粒的质量标准研究[J].成都中医药大学学报,2012,35(3):50-52. |
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| 作者姓名： | 赵小勤 蒲旭峰 |
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| 作者单位： | 1. 成都中医药大学药学院,四川成都,611137
2. 成都市食品药品检测中心,四川成都,610045 |
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| 基金项目： | 国家药典委员会经费支持项目 |
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| 摘 要： | 目的:建立完善独活寄生颗粒的质量控制标准。方法:以薄层色谱法对处方中的独活、秦艽、地黄进行定性鉴别;以高效液相色谱法对秦艽中的龙胆苦苷进行含量测定。结果:在薄层色谱中均可检出独活、秦艽、地黄的特征斑点;龙胆苦苷在0.6408～9.612μg间线性关系良好,r=0.9994,平均加样回收率为99.91%,RSD=1.3%,结论:本方法简便可行、重复性好,可用于独活寄生丸的质量控制。
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| 关 键 词： | 独活寄生丸 质量标准 蛇床子素 薄层色谱法 高效液色谱法 |
Study on Quality Standard for Du-huo-ji-sheng Granules |
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| ZHAO Xiao-qin
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PU Xu-feng.Study on Quality Standard for Du-huo-ji-sheng Granules[J].Journal of Chengdu University of Traditional Chinese Medicine,2012,35(3):50-52. |
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| Authors: | ZHAO Xiao-qin PU Xu-feng |
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| Institution: | 1. Chengdu University Of TCM, 2. Chengdu Food And Drug Testing Center ) |
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| Abstract: | Objective： To establish and optimize the quality control standard of Duhuojisheng Granules. Methods： The medic- inal Radix Angelicae Biseratae, Radix Gentianae Marcrophyllae and Radix Rehmanniae Preparata were identified by TLC. High per- formance liquid chromatography （HPLC） was used to determine the content of Gentiopicroside in Radix Gentianae Marcrophyllae. Re- suits： The herbs of preparation could be identified by TLC. Gentiopicroside showed a good linear relationship at a range of 0. 6408 - 9. 612 μg, r = 0. 9994, and the average recovery was 99. 91% , RSD = 1.3%. Conclusion： The methods were available with a good reproducibility and can controI the quality of this preparation effectively. |
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| Keywords: | Du-huo-ji-sheng granules quality standard gentiopicroside TLC HPLC |
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