| 益气口服液的制备及质量控制 |
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| 引用本文： | 殷金华,黄富宏,张树倩. 益气口服液的制备及质量控制[J]. 中国中医药信息杂志, 2010, 17(9): 48-49. DOI: 10.3969/j.issn.1005-5304.2010.09.021 |
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| 作者姓名： | 殷金华 黄富宏 张树倩 |
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| 作者单位： | 扬州市第一人民医院,江苏,扬州,225001 |
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| 摘 要： | 目的建立益气口服液的制备工艺及质量控制方法。方法采用离心滤过法制备口服液。采用薄层色谱法对处方中的黄芪进行定性鉴别;以无水葡萄糖为含量测定指标,用紫外分光光度法测定制剂中总多糖的含量。结果薄层色谱斑点清晰;无水葡萄糖质量浓度在17～85μg/mL范围内呈良好线性关系(r=0.9992),平均回收率为99.07%,RSD=1.53%(n=6)。结论该制剂制备工艺合理,拟定的鉴别及含量测定方法操作简便可行、准确可靠,可用于益气口服液的质量控制。
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| 关 键 词： | 益气口服液 薄层色谱法 紫外分光光度法 质量控制 |
The Preparation and Quality Control of Yiqi Oral Liquid |
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| YIN Jing-hua,HUANG Fu-hong,ZHANG Shu-qian. The Preparation and Quality Control of Yiqi Oral Liquid[J]. Chinese Journal of Information on Traditional Chinese Medicine, 2010, 17(9): 48-49. DOI: 10.3969/j.issn.1005-5304.2010.09.021 |
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| Authors: | YIN Jing-hua HUANG Fu-hong ZHANG Shu-qian |
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| Affiliation: | (The First People＇s Hospital ofYangzhou, Yangzhou 225001, China) |
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| Abstract: | Objective To establish the preparation process and quality control method of Yiqi Oral Liquid. Methods The oral liquid was made by centrifugal filtration. Radix Astragali was identified by thin-layer chromatography （TLC） method. With anhydrous glucose as a standard, the content of polysaccharide was determined by UV-spectrum. Results The TLC spots developed was fairly clear. The content of anhydrous glucose showed good linear relationship over the range of 17-85 μg/mL （r =0.999 2）. The average recovery was 99.07% with RSD of 1.53% （n =6）. Conclusion The method of preparation is reasonable. The method of identification and content determination is simple and accurate. It can be used for the quality control of Yiqi Oral Liquid. |
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| Keywords: | Yiqi Oral Liquid TLC UV-spectrum quality control |
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