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| 高效液相色谱法测定更年舒片中淫羊藿苷的含量 | |
| 引用本文： | 杨春杰,刘永,孟祥松.高效液相色谱法测定更年舒片中淫羊藿苷的含量[J].世界中西医结合杂志,2010,5(4):313-314. |
| 作者姓名： | 杨春杰 刘永 孟祥松 |
| 作者单位： | 1. 安徽济人药业有限公司,安徽,亳州,236800 2. 安徽省药物研究所,安徽,合肥,230022 3. 安徽省亳州市药品检验所,安徽,亳州,236800 |
| 摘 要： | 目的建立更年舒片中淫羊藿苷的含量测定方法。方法采用高效液相色谱法,以C18色谱柱(5μm,4.6 mm×250 mm);乙腈-水(30∶70)为流动相;流速为1.0 mL.min-1,检测波长为270 nm。结果淫羊藿苷在0.092μg~1.472μg范围内呈良好的线性关系,r=0.999 7。平均回收率为101.4%,RSD为1.0%。结论该方法简单、灵敏度高,可用于更年舒片中淫羊藿苷的含量测定。 |
| 关 键 词： | 更年舒片 淫羊藿苷 高效液相色谱法 含量测定 |
Determination of Icariin Content in Gengnianshu Tables by HPLC |
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| YANG Chun-jie,LIU Yong,MENG Xiang-song.Determination of Icariin Content in Gengnianshu Tables by HPLC[J].World Journal Of Integrated Traditional and Wesrern Medicine,2010,5(4):313-314. | |
| Authors: | YANG Chun-jie LIU Yong MENG Xiang-song |
| Institution: | YANG Chun-jie1,LIU Yong2,MENG Xiang-song3 (1.Anhui Jiren Pharmaceutical Industrial Co.Ltd.,Bozhou Anhui 236800,2.Anhui Pharmaceutical Institute,Hefei Anhui 230022,3.Anhuai Bozhou Drug Control Institute,Bozhou Anhui 236800) |
| Abstract: | Objective To develop a method for the determination of icariin content in gengnianshu tables.Methods HPLC method was adopted,in which C18 column（5 μm,4.6 mm×250 mm）was used,acetonitrile-water（30∶70）was taken as a mobile phase,the flow rate was 1.0 mL·min-1,and the detecting wavelength was 270 nm.Results The good linear range of icariin was displayed in the range of 0.092 μg~1.472 μg,r=0.999 7.The average recovery was 101.4%.Conclusion The method is simple in operation and high in sensitivity and is applicable for icariin content detection in gengnianshu tablets. |
| Keywords: | Gengnianshu Table Icariin HPLC Content Determination |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |