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中草药制剂的回收乙醇中杂质的去除方法探讨
引用本文:蒋三元,曾志坚,林传辉,罗浩章,梁永广.中草药制剂的回收乙醇中杂质的去除方法探讨[J].中国医药导报,2008,5(5):33-34.
作者姓名:蒋三元  曾志坚  林传辉  罗浩章  梁永广
作者单位:1. 广东省江门市新会区中医院,广东江门,529100
2. 广东省江门市药品检验所,广东江门,529000
3. 广东省江门市新会区司前镇卫生院,广东江门,529159
摘    要:目的:探讨中草药制剂的回收乙醇中杂质的去除方法。方法:将回收乙醇进行初步的除杂质实验,选择较好的除杂质方法,再以正交法对其进行优选,并对优选方法加以验证。结果:每1000ml回收乙醇中加入5%高锰酸钾溶液6ml,静置30min,然后加入活性炭6g,再静置30min,滤过,蒸馏,收集蒸馏液作相应的检验,各项指标均能达到规定要求。结论:该方法可有效除去中草药制剂回收乙醇中的杂质,提高其质量。

关 键 词:中草药制剂  回收乙醇  除杂质方法
文章编号:1673-7210(2008)02(b)-033-02
修稿时间:2007年12月21

Study on the removal of impurities in recycled ethanol of medicinal herb preparations
JIANG San-yuan ZENG Zhi-jian LIN Chuan-hui LUO Hao-zhang LIANG Yong-guang.Study on the removal of impurities in recycled ethanol of medicinal herb preparations[J].China Medical Herald,2008,5(5):33-34.
Authors:JIANG San-yuan ZENG Zhi-jian LIN Chuan-hui LUO Hao-zhang LIANG Yong-guang
Institution:JIANG San-yuan~1 ZENG Zhi-jian~2 LIN Chuan-hui~3 LUO Hao-zhang~2 LIANG Yong-guang~1
Abstract:Objective:To discuss the method about how to remove the impurities in recycled ethanol of medicinal herb preparations.Methods:The initial test was carried out to remove the impurities in recycled ethanol and the better method was chosen which would be verified by orthogonal test.Results:1 000 ml of recycled ethanol liquor solution was put in 6 ml of 5%KMNO_4,standing for 30 min and 6 g of activated carbon,standing for 30 min again.Then it was filtrated and dis- tilled,and the distilled ethanol was collected to make corresponding tests.All indexes of ethanol tests had reached regu- lary request.Conclusion:This method can remove the impurities in recycled ethanol of medicinal herb preparations.The quality of recycled ethanol is improved.
Keywords:Medicinal herb preparation  Recycled ethanol  Removal of impurities
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