| 肾特康胶囊质量控制方法的研究 |
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| 引用本文： | 胡雪来,王爱良,吴泽君,刘水平,刘光喜,彭小菊,周红玲. 肾特康胶囊质量控制方法的研究[J]. 中国药房, 2006, 17(3): 189-191 |
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| 作者姓名： | 胡雪来 王爱良 吴泽君 刘水平 刘光喜 彭小菊 周红玲 |
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| 作者单位： | 1. 湖南中医学院附属第三医院药剂科,株洲市,412000
2. 湖南株洲市药品检验所,株洲市,412008 |
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| 摘 要： | 目的建立肾特康胶囊的质量控制方法。方法用薄层色谱法对肾特康胶囊中的黄芪、人参、发酵虫草菌粉进行定性鉴别;采用高效液相色谱法测定肾特康胶囊中盐酸小檗碱的含量。结果薄层色谱中斑点清晰,易于识别;盐酸小檗碱线性范围为0.0351μg~0.263μg(r=0.9999),平均回收率为98.88%,RSD=1.07%(n=5)。结论本方法简便,灵敏度高,可有效控制肾特康胶囊的质量。
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| 关 键 词： | 肾特康胶囊 薄层色谱法 高效液相色谱法 盐酸小檗碱 |
| 文章编号： | 1001-0408(2006)03-0189-03 |
| 收稿时间： | 2005-01-15 |
| 修稿时间： | 2005-03-31 |
Quality Control of Shentekang Capsules |
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| HU Xuelai,WANG Ailiang,WU Zejun,LIU Shuiping,LIU Guangxi,PENG Xiaoju,ZHOU Hongling. Quality Control of Shentekang Capsules[J]. China Pharmacy, 2006, 17(3): 189-191 |
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| Authors: | HU Xuelai WANG Ailiang WU Zejun LIU Shuiping LIU Guangxi PENG Xiaoju ZHOU Hongling |
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| Affiliation: | 1.Dept of Pharmacy, The Third Affiliated Hospital, Humm College of TCM, Zhuzhou 412000, China;2.Zhuzhou Institute of Drug Test, Zhuzhou 412008,China |
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| Abstract: | OBJECTIVE:To establish a method for quality control of Shentekang capsules.METHODS:The Radix astragali,Radix ginseng,fermental cordyceps powder in this medicine were identified by TLC.The contents of berberine hydrochloride in this medicine were measured by HPLC.RESULTS:The spots in TLC were clear and well distinguished.The method was linear within a range of0.0351～0.263μg for berberine hydrochloride(r=0.9999),the average recovery was98.88%,and RSD=1.07%(n=5).CONCLUSIONS:The method is simple,sensitive and accurate,which can be used to control the quality of Shentekang capsules. |
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| Keywords: | Shcntckang capsules TLC HPLC Berberine hydrochloride |
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