云南傣药竹叶兰化学成分的研究 |
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作者姓名: | 李玉鹏 翁瑞旋 陶永生 李双 王娟 黄荣 文小玲 张桂花 |
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作者单位: | 1. 昆明医科大学药学院暨云南省天然药物药理重点实验室 |
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基金项目: | 基金: 国家自然科学基金资助项目(21202066); 云南省科技厅-昆明医科大学联合专项基金资助项目(K13201233); 云南省教育厅科学研究基金资助项目(2015Y151,2016ZDX050); |
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摘 要: | 目的 研究云南傣药竹叶兰化学成分,发现其活性成分.方法 竹叶兰全草经溶剂提取、硅胶柱层析和Sephadex LH-20柱层析进行分离纯化,波谱分析(核磁共振氢谱、碳谱、和质谱)确定结构.结果 从该药用植物分离并鉴定了8个化合物,分别为:(1)7-hydroxy-2,4-dimethoxy-9,10-dihydrophenanthrene;(2)coelonin;(3)4,7-dihydro-xy-2-methoxy-9,10-dihydrophenanthrene;(4)ephemeranthoquinone;(5)densiflorol B;(6)4-(3-hydroxyphenyl)-2-butanone;(7)stigmasterol;(8)β-sitosterol.结论 化合物6为首次从竹叶兰中得到.
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关 键 词: | 竹叶兰 药用植物 化学成分 |
收稿时间: | 2016-03-14 |
Study on the Chemical Constituents of Arundina graminifolia |
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Abstract: | Objective To study the chemical constituents from the flowers of Arundina graminifolia and to find its bioactive compounds. Methods The compounds were extracted by 95% alcohol and isolated by column chromatography on silica gel and Sephadex LH-20. The structures were identified by spectroscopic analysis(1H NMR,13 CNMR and EIMS). Results Eight compounds were obtained and identified as(1) 7-hydroxy-2,4-dimethoxy-9,10-dihydrophenanthrene;(2)coelonin;(3)4,7-dihydroxy-2-methoxy-9,10-dihydro-phenanthrene;(4)ephemeranthoquinone;(5)densiflorol B;(6)4-(3-hydroxyphenyl)-2-butanone;(7)stigmasterol,(8)β-sitosterol.Conclusion Among them, compound 6 is discovered for the first time from the plant. |
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