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盆炎净片的质量控制
引用本文:尹伟,岳春华,雷伟,刘柄成,黄丹.盆炎净片的质量控制[J].中南药学,2007,5(3):246-249.
作者姓名:尹伟  岳春华  雷伟  刘柄成  黄丹
作者单位:[1]浏阳市妇幼保健院,长沙410300 [2]湖南省中医药研究院中药研究所,长沙410013 [3]湖南中医药大学,长沙410007 [4]石门县中医院,湖南常德415000
摘    要:目的制定盆炎净片的质量控制标准。方法采用薄层色谱法鉴别忍冬藤、蒲公英、赤芍、狗脊,高效液相色谱法测定芍药苷的含量。结果薄层斑点清晰,阴性样品无干扰;含量测定平均回收率为97.88%,RSD为0.80%。结论所建方法准确、重复性好,可有效控制该制剂的质量。

关 键 词:盆炎净片  芍药苷  忍冬藤  蒲公英  赤芍  狗脊  质量标准  高效液相色谱法
文章编号:1672-2981(2007)03-0246-04
修稿时间:2007-03-012007-03-29

Quality control of Penyanjing tablets
YIN Wei,YUE Chun-hua,LEI Wei,LIU Bing-cheng,HUANG Dan.Quality control of Penyanjing tablets[J].Central South Pharmacy,2007,5(3):246-249.
Authors:YIN Wei  YUE Chun-hua  LEI Wei  LIU Bing-cheng  HUANG Dan
Institution:1. Liuyang Maternal and Child Health Hospital, Changsha 410300; 2. Institute of Chinese Materia Medica, Hunan Academy of Traditional Chinese Medicine, Changsha 410013; 3. Hunan University of Traditional Chinese Medicine, Changsha 410007; 4. Shimen Traditional Chinese Medicine Hospital, Changde Hunan 415000
Abstract:Objective To establish the quality control criteria for Penyanjing tablets.Methods Thin-layer chromatography(TLC) was used to identify Caulis Lonicerae Japonicae,Herba Taraxaci,Radix Paeoniae Rubra,and Rhizoma Cibotii,and the content of Paeoniflorin was determined by HPLC.Results The TLC spots developed were fairly clear,and the average recovery of Paeoniflorin was 97.88% with RSD of 0.80%.Conclusion The method is accurate and reproducible,and can effectively control Penyanjing tablets.
Keywords:Penyanjing tablets  Paeoniflorin  Caulis Lonicerae Japonicae  Herba Taraxaci  Radix Paeoniae Rubra  Rhi zoma Cibotii  quality criteria  HPLC
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