| 用大孔吸附树脂分离菝葜总皂苷的条件优化 |
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| 引用本文： | 舒孝顺高中洪,杨祥良.用大孔吸附树脂分离菝葜总皂苷的条件优化[J].中国中药杂志,2005,30(1):30-33. |
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| 作者姓名： | 舒孝顺高中洪 杨祥良 |
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| 作者单位： | 华中科技大学,生命科学与技术学院,药物研究所,湖北,武汉,430074 |
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| 摘 要： | 目的 :开发一种高效、实用的提取、分离菝葜总皂苷的技术。方法 :以总皂苷吸附量和解吸率为指标 ,对 4种树脂进行了筛选 ,并研究吸附与解吸优化条件。结果 :所选出的非极性大孔树脂HPD10 0 ,在实验条件下对菝葜总皂苷的吸附量和解吸率分别达到 16mg·mL-1和 90 %。结论 :HPD10 0型树脂能很好地用于吸附、分离菝葜总皂苷。
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| 关 键 词： | 菝葜 总皂苷 大孔树脂 吸附分离 |
| 文章编号： | 1001-5302(2005)01-0030-04 |
| 收稿时间： | 2003/11/15 0:00:00 |
Optimization of purification conditions for with macroporous adsorption resin total saponins from Smilax china |
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| SHU Xiao-shun;GAO Zhong-hong;YANG Xiang-liang.Optimization of purification conditions for with macroporous adsorption resin total saponins from Smilax china[J].China Journal of Chinese Materia Medica,2005,30(1):30-33. |
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| Authors: | SHU Xiao-shun;GAO Zhong-hong;YANG Xiang-liang |
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| Institution: | Institute of Materia Medica, Huazhong University of Science and Technology, Wuhan 430074, China. sxs732@sohu.com |
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| Abstract: | Objective: To develop a with high efficiency and practicality for separating and purifying total steroidal saponins from Smilax china. Method: Using adsorption capacity and desorption rate of total steroidal saponins as the primary screening index, four resins were surveyed, and the optimized conditions of adsorption and desorption of total steroidal saponins were studied. Result: The adsorption capacity and desorption rate of total steroidal saponins reached 16 mg·mL-1 and 90% respectively for macroporous resin HPD100 chosen. Conclusion: Macroporous resin HPD100 could be well used in separating and purifying total steroidal saponins from S. china. |
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| Keywords: | Smilax china total steroidal saponins macroporous adsorption resin purification |
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