| 乌拉尔甘草中的一个新三萜皂苷成分 |
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| 引用本文： | 张慧,王世盛,李伟,王亚琴,薛兴亚,梁鑫淼. 乌拉尔甘草中的一个新三萜皂苷成分[J]. 世界科学技术, 2009, 11(2): 253-256 |
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| 作者姓名： | 张慧 王世盛 李伟 王亚琴 薛兴亚 梁鑫淼 |
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| 作者单位： | 张慧,李伟,王亚琴,薛兴亚,梁鑫淼,Hui Zhang,Wei Li,Yaqin Wang,Xingya Xue,Xinmiao Liang(中科院大连化学物理研究所分析化学分离科学重点实验室,大连,116023);王世盛,Shisheng Wang(大连理工大学化工学院精细化工国家重点实验室,大连,116012) |
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| 基金项目： | 辽宁省科技计划重大项目 |
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| 摘 要： | 目的：研究乌拉尔甘草（Glycyrrhiza uranlelnsis Fisch.）的化学成分。方法：采用制备型高效液相色谱分离，应用波谱方法进行结构鉴定。结果：从甘草中共分离出11个黄酮和4个三萜皂苷类化合物，其中一个三萜皂苷（S3）为新化合物。结论：通过ESI-MS，UV，IR和NMR分析，将新三萜皂苷的结构鉴定为22β-乙酰基甘草醛（22β-acetoxyl-glycyrrhaldehyde）。
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| 关 键 词： | 乌拉尔甘草 三萜皂苷 22β-乙酰基甘草醛 |
New Oleanane-type Triterpene Glycoside in Glycyrrhiza uralensis Fisch |
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| Hui Zhang,Shisheng Wang,Wei Li,Yaqin Wang,Xingya Xue,Xinmiao Liang. New Oleanane-type Triterpene Glycoside in Glycyrrhiza uralensis Fisch[J]. World Science and Technology(Modernization of Traditional Chinese Medicine), 2009, 11(2): 253-256 |
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| Authors: | Hui Zhang Shisheng Wang Wei Li Yaqin Wang Xingya Xue Xinmiao Liang |
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| Affiliation: | Hui Zhang, Shisheng Wang, Wei Li, Yaqin Wang,Xingya Xue,Xinmiao Lian(1.Key Lab of Separation Science for Analytical Chemistry, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, No. 457 Zhongshan Road, Dalian 116023, China;2.State Key Laboratory of Fine Chemicals, School of Chemical Engineering, Dalian University of Technology, Dalian 116012, China) |
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| Abstract: | This is a study to investigate the chemical constituents contained in the roots of Glycyrrhiza uranlelnsis Fisch. In the study, constituents were isolated using preparative HPLC, and the structures of the isolated compounds identified by spectral evidence. A new oleanane-type triterpenoid saponin （S3） and eleven known compounds were derived from the experiment. The new licorice saponin （S3） was identified as 22β-acetoxyl-glycyrrhaldehyde based on MS, UV, IR and NMR spectroscopic data. |
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| Keywords: | Glycyrrhiza uralensis Fisch. tritepenoid saponin 22β-acetoxyl-glycyrrhaldehyde |
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