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薄层扫描法测定安宫宁胶囊中千层纸甲素A的含量
引用本文:余子川. 薄层扫描法测定安宫宁胶囊中千层纸甲素A的含量[J]. 中国药学杂志, 2002, 22(10): 598-599
作者姓名:余子川
作者单位:湖北中医学院药学系,湖北 武汉430061
摘    要: 目的:建立安宫宁胶囊中千层纸甲素A的含量测定方法。方法:测定波长λS=315 nm,参比波长λR=360 nm,展开剂为苯-甲醇-冰醋酸(95∶5∶0.2)。结果:千层纸甲素A的平均回收率为96.96%,RSD=2.1%。结论:该方法简便、快速、准确,可用于安宫宁胶囊的质量控制。

关 键 词:安宫宁胶囊  千层纸甲素A
收稿时间:2002-02-28;

Determination of oroxylin-A in Angongning capsules by TLC-scanning
YU Zi-Chuan,. Determination of oroxylin-A in Angongning capsules by TLC-scanning[J]. Chinese Pharmaceutical Journal, 2002, 22(10): 598-599
Authors:YU Zi-Chuan  
Affiliation:Department of Medicine, Hubei College of Traditional Chinese Medicine, Hubei Wuhan 430061
Abstract:OBJECTIVE To establish a method for determining the content of oroxylin-A in Angongning capsules.METHODS The sample and reference wavelength was 315 nm and 365 nm respectively. The mobile phase was benzene-methanol-glacial acetic acid (95∶5∶0.2).RESULTS The rate of average recovery of oroxylin-A was 96.96%, and RSD=2.1%.CONCLUSIONS The method is sample, rapid, accurate and can be used for the quality controle of Angongnin capsules.
Keywords:Angongning capsules  oroxylin-A  TLC-scanning
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