| 高效液相色谱法测定通降胃灵片中橙皮苷的含量 |
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| 引用本文： | 彭洁,刘启斌,许汉香,王志萍. 高效液相色谱法测定通降胃灵片中橙皮苷的含量[J]. 中国药学杂志, 2002, 22(4): 214-215 |
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| 作者姓名： | 彭洁 刘启斌 许汉香 王志萍 |
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| 作者单位： | 1.荆州市中医院，湖北 荆州434000；2.荆州市药品检验所，湖北 荆州434000 |
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| 摘 要： | 目的：建立通降胃灵片中橙皮苷的HPLC含量测定方法。方法：用Nova?pak C18柱，流动相为甲醇-醋酸-水(35∶4∶61）在283 nm波长处检测。结果：线性范围为0.65～1.3 μg 。橙皮苷的加样回收率为99.03%,RSD为1.14%(n=5)。结论：方法简便、快速，精密度和稳定性良好，适合于通降胃灵片生产的质量控制。
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| 关 键 词： | 通降胃灵片 橙皮苷 含量测定 高效液相色谱法 |
| 收稿时间： | 2001-06-19; |
Determination of hesperidin in Tongjiangweiling tablet by HPLC |
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| PENG Jie,LIU Qi-Bing,XU Han-Xiang,et al. Determination of hesperidin in Tongjiangweiling tablet by HPLC[J]. Chinese Pharmaceutical Journal, 2002, 22(4): 214-215 |
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| Authors: | PENG Jie LIU Qi-Bing XU Han-Xiang et al |
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| Affiliation: | Traditional Chinese Medicine Hospital of Jinzhou, Hubei Jinzhou 434000 |
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| Abstract: | ABSTRACTOBJECTIVE To establish an HPLC method for determination of hesperidin in Tongjiangweiling tablet.METHODS A Nova-pak C18 column was used, the mobile phase was methanol-acetic acid-water (35∶4∶61), detection wavelength was 283 nm.RESULTS The detection ranges was 0.65～1.3 μg. The average recovery of hesperidin was 99.03% (RSD=1.14%, n=5).CONCLUSIONS HPLC method cloud be used for quality control in the production of Tongjiangweiling tablet. |
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| Keywords: | hesperdin Tongjiangweiling tablet assay HPLC scanning |
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