| HPLC法测定稀戊二醛溶液中戊二醛含量 |
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| 引用本文： | 杜建红,徐小平,王艳丽,郄革红,赵晓娟.HPLC法测定稀戊二醛溶液中戊二醛含量[J].北方药学,2014,0(4):2-3. |
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| 作者姓名： | 杜建红 徐小平 王艳丽 郄革红 赵晓娟 |
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| 作者单位： | 杜建红 (成都军区联勤部药品仪器检验所 成都 610017)； 徐小平 (四川大学华西药学院 成都 610041)； 王艳丽 (成都军区联勤部药品仪器检验所 成都 610017)； 郄革红 (成都军区联勤部药品仪器检验所 成都 610017)； 赵晓娟 (成都军区联勤部药品仪器检验所 成都 610017)； |
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| 基金项目： | 基金项目：军队医疗机构制剂标准提高科研专项课题面上项目,编号：13ZJZ04-2. |
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| 摘 要： | 目的：建立HPLC法测定稀戊二醛溶液中戊二醛含量的方法。方法：采用AichromBond-AQ C18色谱柱（4.6mm＆#215;150mm，5μm），流动相：甲醇∶水（50∶50），流速0.5ml/min，检测波长235nm，进样量20μl。结果：戊二醛在51.6～1010.4μg/ml范围内时，与峰面积呈良好的线性关系（r=0.9992），平均回收率为101.1%。结论：本法操作简便，灵敏度高，重复性好，可用于稀戊二醛溶液中戊二醛的含量控制。
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| 关 键 词： | 稀戊二醛溶液 戊二醛 高效液相色谱法 测定 |
Determination of Glutaraldehyde in Dilute Glutaraldehyde Solution by HPLC |
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| Du Jianhong Xu Xiaoping Wang Yanli Qie Gehong Zhao Xiaojuan.Determination of Glutaraldehyde in Dilute Glutaraldehyde Solution by HPLC[J].BEIFANG YAOXUE,2014,0(4):2-3. |
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| Authors: | Du Jianhong Xu Xiaoping Wang Yanli Qie Gehong Zhao Xiaojuan |
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| Institution: | Du Jianhong Xu Xiaoping Wang Yanli Qie Gehong Zhao Xiaojuan (1.Institute for Drug and Instrument Control of Chengdu Military Region, Chengdu 610017, China; 2.West China School of Pharmacy Sichuan University, Chengdu 610041, China) |
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| Abstract: | Objective：To establish an HPLC method for the determination of Glutaraldehyde in Dilute Glutaraldehyde Solution.Method：An AichromBond-AQ C18 column（4.6mm＆#215;150mm,5μm） was used,the mobile phase was Methanol-Water（50∶50）.The flow rate was 0.5 ml/min,the detection wavelength was 235nm and the injection volume was 20μl. Results： Within the range from 51.6 to 1010.4μg/ml,Glutaraldehyde presented a good relationship between the injected amounts and peak areas （r=0.9992）.The average recovery was 101.1%.Conclusion： The method was easy to operate, with sensitive,and reproducible. It can be used for the quality control of Glutaraldehyde in Dilute Glutaraldehyde Solution. |
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| Keywords: | Glutaraldehyde Dilute Glutaraldehyde Solution HPLC Detemination |
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