| 六味芦荟膏质量标准研究 |
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| 引用本文： | 梁其冰,朱毅,黄守良.六味芦荟膏质量标准研究[J].中国药房,2008,19(18):1388-1390. |
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| 作者姓名： | 梁其冰 朱毅 黄守良 |
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| 作者单位： | 梁其冰 (海南省药物研究所,海口市,570216)； 朱毅 (海南省药物研究所,海口市,570216)； 黄守良 (海南省药物研究所,海口市,570216)； |
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| 基金项目： | 国家高技术研究发展计划(863计划) |
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| 摘 要： | 目的:建立六味芦荟膏的质量标准。方法:采用薄层色谱法对方中黄连、虎杖、芦荟进行定性鉴别;采用高效液相色谱法对芦荟大黄素进行含量测定。结果:定性鉴别试验特征明显、专属性强、阴性无干扰;芦荟大黄素检测浓度在1~20μg.mL-1范围内与峰面积积分值呈良好线性关系(r=0.9997);平均加样回收率为95.94%,RSD=1.1%(n=6)。结论:所建标准可用于六味芦荟膏的质量控制。
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| 关 键 词： | 六味芦荟膏 质量标准 薄层色谱法 高效液相色谱法 |
Quality Standard of Liuweiluhui Ointment |
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| LIANG Qi-bing,ZHU Yi,HUANG Shou-liang.Quality Standard of Liuweiluhui Ointment[J].China Pharmacy,2008,19(18):1388-1390. |
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| Authors: | LIANG Qi-bing ZHU Yi HUANG Shou-liang |
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| Institution: | (Hainan Institute of Pharmaceutical Research, Haikou 570216, China) |
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| Abstract: | OBJECTIVE： To establish the quality standard of Liuweiluhui ointment. METHODS： Phizoma Coptidis, Rhizoma Et Radix Polygoni Cuspidati and Aloe in Liuweiluhui ointment were identified qualitatively by TLC. The content of Aloe - emodin in Liuweiluhui ointment was determined by HPLC. RESULTS： The TLC spots were clear and specific yet without the interference of negative samples. The linear range of Aloe-emodin was 1-20μg· mL^-1（r = 0.999 7） . The average recovery was 95.94% （RSD = 1.1%, n = 6）. CONCLUSION： The established standard is suitable for the quality control of Liuweiluhui ointment. |
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| Keywords: | Liuweiluhui ointment Quality standard TLC HPLC |
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