| GC法测定肛安栓中冰片的含量 |
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| 引用本文： | 高辉,徐丽华.GC法测定肛安栓中冰片的含量[J].齐鲁药事,2012,31(3):145-146. |
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| 作者姓名： | 高辉 徐丽华 |
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| 作者单位： | 山东省食品药品检验所,山东,济南,250101 |
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| 摘 要： | 目的采用气相色谱法测定肛安栓中冰片的含量。方法 Agilent HP-FFAP石英毛细管柱(0.25 mm×30.0m,0.25μm),柱温130℃,进样口温度180℃;检测器温度230℃;氢离子火焰检测器;恒流;分流比40∶1。结果冰片的进样量在0.058～1.450 0μg之间与峰面积呈良好的线性关系,相关系数r=0.999 97,平均加样回收率为98.30%,RSD=1.70%(n=6)。结论本法简便、准确,可用于肛安栓中冰片的含量测定。
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| 关 键 词： | 肛安栓 冰片 气相色谱法 含量测定 |
Determination of borneol in Gangan Suppositories by GC |
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| GAO Hui
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XU Li-hua.Determination of borneol in Gangan Suppositories by GC[J].qilu pharmaceutical affairs,2012,31(3):145-146. |
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| Authors: | GAO Hui XU Li-hua |
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| Institution: | ( Shandong Institute for Food and Drug Control,Jinan 250101, China) |
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| Abstract: | Objective To establish a GC method for the determination of borneol in Gangan Suppositories. Methods Agi- lent HP - FFAP capillary column （ 0.25 mm×30.0 m,0.25 um ） was adopted with a flame ionization detector. The column tem- perature was 130 ℃ ,the inlet temperature was 180 ℃ and the deteetor temperature was 230 ℃. The constant flow mode was conducted with the split ratio of 40： 1. Results The linear range of borneol was 0. 058 - 1. 450 0 ug （ r = 0. 999 97 ）. The average recovery was 98.30% and the RSD was 1.70% （ n = 6）. Conclusion The method was simple and accurate, and it can be used for the determination of borneol in Gangan Suppositories. |
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| Keywords: | Gangan Suppositories Borneol GC Determination |
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