| 流感丸中乌头碱的限量检查及HPLC含量测定方法的建立 |
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| 引用本文： | 刘高宏,魏立莉. 流感丸中乌头碱的限量检查及HPLC含量测定方法的建立[J]. 西部中医药, 2016, 0(11): 24-26. DOI: 10.3969/j.issn.1004-6852.2016.11.008 |
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| 作者姓名： | 刘高宏 魏立莉 |
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| 作者单位： | 甘肃省中医院,甘肃兰州,730050 |
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| 摘 要： | 目的:建立流感丸中乌头碱的限量检查及HPLC含量测定方法。方法:采用薄层色谱法对流感丸中乌头碱进行限量检查;采用高效液相色谱法测定流感丸中乌头碱的含量。结果:薄层色谱方法简便、专属性强,乌头碱在8.0~20μg/m L范围内呈良好线性关系,平均加样回收率为98.85%(RSD%=1.43%)。结论:该法稳定、快速、简便,结果准确、可靠,可用于流感丸中乌头碱的限量检查及含量测定。
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| 关 键 词： | 流感丸 乌头碱 限量检查 高效液相色谱法 |
Construction of Aconitine Limited Inspection and HPLC Determination Method in LiuGanWan |
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| Abstract: | Objective:To establish the aconitine limited inspection and HPLC determination method in LiuCanWan.Methods:Thin-layer chromatography (TLC) was used for the aconitine limited inspection in LiuGanWan.High performance liquid chromatography (HPLC) method was used to determine the aconitine content level in LiuGanWan.Results:TLC was simple and convenient with strong specificity,aconitine in 8.0 ～20 μg/mL had good linear relationship,and the average sample recovery rate was 98.85％(RSD％=l.43％).Conclusion:This method is stable,fast,simple and convenient,accurate,reliable and can be used for the aconitine limited inspection and content determination in LiuGanWan. |
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| Keywords: | LiuGanWan aconitine limited inspection HPLC |
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