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不同来源国产血竭的薄层色谱和紫外光谱鉴别
引用本文:孙胜利,宓鹤鸣,吴眚倩,姚庆芳,胡因铭,郑有顺. 不同来源国产血竭的薄层色谱和紫外光谱鉴别[J]. 中草药, 2002, 33(11): 1033-1036
作者姓名:孙胜利  宓鹤鸣  吴眚倩  姚庆芳  胡因铭  郑有顺
作者单位:1. 第二军医大学药学院药物分析教研室,上海,200433
2. 广东名盛药业有限公司开发部,广东,广州,510240
摘    要:目的:比较6种不同来源国产血竭的质量差异。方法:以剑叶龙血树含皮及木质部为原料,采用回流提取、索氏提取,超声提取,低温膨化提取,并与市售的通过传统工艺提取的云南血竭和海南血竭为对照,对它们进行薄层层析和紫外光谱鉴别。结果:薄层对应斑点基本相同,紫外光谱基本一致。结论:6种不同来源的国产血竭的成分基本一致,而以龙血素C作为评价指标,其质量存在一定差异。

关 键 词:国产血竭 薄层色谱 紫外光谱 原产地 药材鉴定
文章编号:0253-2670(2002)11-1033-04
收稿时间:2002-10-12
修稿时间:2002-10-12

Identification of Resina Draconis from different source by TLC and UV spectrophotometry
SUN Sheng li,MI He ming,WU Sheng qian,YAO Qing fang,HU Yin ming and ZHENG You shun. Identification of Resina Draconis from different source by TLC and UV spectrophotometry[J]. Chinese Traditional and Herbal Drugs, 2002, 33(11): 1033-1036
Authors:SUN Sheng li  MI He ming  WU Sheng qian  YAO Qing fang  HU Yin ming  ZHENG You shun
Affiliation:Department of Pharmaceutical Analysis, College of Pharmacy, Second Military Medical University, Shanghai 200433, China;Department of Pharmaceutical Analysis, College of Pharmacy, Second Military Medical University, Shanghai 200433, China;Department of Pharmaceutical Analysis, College of Pharmacy, Second Military Medical University, Shanghai 200433, China;Department of Development, Guangdong Mingsheng Pharmaceutical Co., Ltd., Guangzhou 510240, China;Department of Development, Guangdong Mingsheng Pharmaceutical Co., Ltd., Guangzhou 510240, China;Department of Development, Guangdong Mingsheng Pharmaceutical Co., Ltd., Guangzhou 510240, China
Abstract:Object To compare the quality difference of six kinds of Resina Draconis. Methods Four kinds of Resina Draconis were extracted by reflux, Soxhlet method, ultrasonic extraction and cryogenic expansion from bark and cylem with fat in Dranaena cochinchinensis (Lour) S. C. Chen and compare with those sold in Yunnan and Hainan, which were identified by TLC and UV spectrophotometry. Results Six kinds of Resina Draconis were identical basically in TLC and UV. Conclusion The components of six kinds of Resina Draconis are identical basically, but there are some differences estimated by loureirin C as evaluate index.
Keywords:Resina Dracoins  TLC  UV
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