| 十八味诃子利尿丸质量标准研究 |
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| 引用本文： | 刘合禄,庄肃农,齐静.十八味诃子利尿丸质量标准研究[J].齐鲁药事,2010,29(4):213-215. |
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| 作者姓名： | 刘合禄 庄肃农 齐静 |
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| 作者单位： | 1. 山东金藏煌药业集团股份有限公司,山东,乐陵,253600
2. 莒县人民医院,山东,日照,276500 |
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| 摘 要： | 目的建立十八味诃子利尿丸的质量控制方法。方法采用TLC法对本品中的小檗皮、姜黄进行薄层鉴别;采用HPLC法对本品中盐酸小檗碱进行含量测定。结果在TLC色谱图中可检出小檗皮、姜黄;盐酸小檗碱在14.88～74.40μg·mL-1范围内呈良好的线性关系(r=0.9998),平均回收率为98.64%,RSD=1.48%。结论所用方法简便、准确,可以用于十八味诃子利尿丸的质量控制。
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| 关 键 词： | 十八味诃子利尿丸 小檗皮 姜黄 盐酸小檗碱 |
Study on quality standard for Shibawei Hezi Liniao Pill |
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| LIU He-lu,ZHUANG Su-nong,QI Jing.Study on quality standard for Shibawei Hezi Liniao Pill[J].qilu pharmaceutical affairs,2010,29(4):213-215. |
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| Authors: | LIU He-lu ZHUANG Su-nong QI Jing |
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| Institution: | (Shandong Jinzanghuang Pharmaceutical Group Co. ,Ltd. ,Leling 253600;1. Ju County People＇s Hospital,Rizhao 276500) |
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| Abstract: | OBJECTIVE To establish the quality standard for Shibawei Hezi Liniao Pill. METHODS Cortex Berberidis, Rhizoma Curcumae Longae were identified by TLC. The content of Berberine Hydrochloride in Cortex Berberidis was determined by HPLC. RESULTS Cortex Berberidis,Rhizoma Curcumae Longae were identified by TLC. Berberine Hydrochloride showed a good linear relationship at the range of 14.88～74.40μg · mL-1 （ r =0. 9998）. The average recovery was 98. 64%, RSD = 1.48%. CONCLUSION The method was simple with good reproducibility and can be used for the quality control of Shibawei Hezi Liniao Pill. |
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| Keywords: | Shibawei Hezi Liniao Pill Cortex Berberidis Rhizoma Curcumae Longae berberine hydrochloride |
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