| 萨木萨克油的质量标准研究 |
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| 引用本文： | 汗克孜·吐尔逊,姜湘英,帕尔哈提·吐尔逊,牙克甫江·尼亚孜,彭小丽. 萨木萨克油的质量标准研究[J]. 西北药学杂志, 2017, 0(1): 24-28. DOI: 10.3969/j.issn.1004-2407.2017.01.007 |
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| 作者姓名： | 汗克孜·吐尔逊 姜湘英 帕尔哈提·吐尔逊 牙克甫江·尼亚孜 彭小丽 |
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| 作者单位： | 1. 新疆巴州食品药品检验所,库尔勒,841000;2. 新疆库尔勒市维吾尔医医院,库尔勒,841000 |
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| 摘 要： | 目的建立萨木萨克油的质量标准。方法采用TLC法鉴别丁香和大蒜;采用HPLC法检测大蒜素的含量。色谱柱:Wondasil C18(150mm×4.6mm,5μm);流动相:甲醇-1mL·L~(-1)甲酸(75∶25);柱温:30℃;流速:1.0mL·min~(-1);检测波长:210nm。结果薄层色谱法对丁香和大蒜的鉴别效果好,重复性好,阴性对照无干扰,其线性范围为9.99~199.85μg·mL~(-1)(r=0.999 8),回收率为100.9%(RSD=1.2%)。结论该方法操作简单、准确、重复性好,可用于萨木萨克油的质量控制。
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| 关 键 词： | 大蒜素 萨木萨克油 薄层色谱法 高效液相色谱法 |
Study on the quality standard of Samusake Oil |
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| Hankiz TURSUN,JIANG Xiangying,Parhat TURSUN,Yakupjan NIYAZ,PENG Xiaoli. Study on the quality standard of Samusake Oil[J]. Northwest Pharmaceutical Journal, 2017, 0(1): 24-28. DOI: 10.3969/j.issn.1004-2407.2017.01.007 |
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| Authors: | Hankiz TURSUN JIANG Xiangying Parhat TURSUN Yakupjan NIYAZ PENG Xiaoli |
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| Abstract: | Objective To establish the quality standard for Samusake Oil .Methods TLC was used for the identification of Caryo‐phylli f los and A llii sativi bulbus .HPLC was used for the determination of allicin .The separation was performed on Wondasil C18 column (150 mm × 4 .6 mm ,5μm) with mobile phase consisting of methanol‐1 mL · L -1 formic acid (75∶25) at a flow rate of 1 .0 mL · min-1 .The oven was 30 ℃ and the detection wavelength was 210 nm .Results The TLC identification of Caryophylli f los and A llii sativi bulbus showed excellent effect and good reproducibility .The negative control showed no interference .The linearity range of allicin was 9 .99‐199 .85 μg·mL -1 (r=0 .999 8) ,and the average recovery was 100 .9% (RSD=1 .2% ) .Conclusion The established method was simple ,accurate and reproducible and could be used for the quality control of Samusake Oil . |
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| Keywords: | allicin Samusake Oil TLC HPLC |
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