| 程序升温气相色谱法测定肌醇的含量 |
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| 引用本文： | 严拯宇,姜新民,黎红梅,胡育筑. 程序升温气相色谱法测定肌醇的含量[J]. 药学与临床研究, 2002, 10(4): 16-18 |
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| 作者姓名： | 严拯宇 姜新民 黎红梅 胡育筑 |
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| 作者单位： | 中国药科大学,南京,210009 |
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| 摘 要： | 目的 :建立程序升温气相色谱法测定肌醇的含量。方法 :将肌醇进行硅烷化处理 ,正己烷提取后 ,以程序升温气相色谱法测定肌醇的含量。结果 :肌醇的重复性试验 RSD为 2 .0 % ;平均回收率为 99.4 %。结果 :该方法操作简便 ,易行 ,线性关系良好
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| 关 键 词： | 程序升温 气相色谱 肌醇 硅烷化 含量测定 |
| 修稿时间： | 2002-06-04 |
Programmed Temperature-GC Determination of Inositol |
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| Yan Zhengyu,Jiang Xinmin,Li Hongmei,Hu Yuzhu China Pharmaceutical University,Nanjing. Programmed Temperature-GC Determination of Inositol[J]. Pharmacertical and Clinical Research, 2002, 10(4): 16-18 |
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| Authors: | Yan Zhengyu Jiang Xinmin Li Hongmei Hu Yuzhu China Pharmaceutical University Nanjing |
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| Affiliation: | Yan Zhengyu,Jiang Xinmin,Li Hongmei,Hu Yuzhu China Pharmaceutical University,Nanjing 210009 |
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| Abstract: | AIM:The purpose is to develop a method for determining the content of inositol. METHOD:After silanization, the inositol was extracted with n hexane and determined by programmed temperature GC. RESULT:The relative standard deviation of the repeatability was 2 0% and the average recovery was 99 4%.CONCLUSION:The method was simple and of good liner relationship. |
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| Keywords: | Programmed temperature GC Inositol Silanization Determination of content |
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