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肠安口服液质量标准的制订
引用本文:万绍晖,单季先,张孝祯. 肠安口服液质量标准的制订[J]. 中药材, 2000, 23(1): 43-44
作者姓名:万绍晖  单季先  张孝祯
作者单位:开封医学高等专科学校,开封,475001
摘    要:目的 制订中药制剂肠安口服液的质量标准。方法:采用薄层层析法硫酸-糠醛法对猪胆汁进行鉴别,薄层扫描法测定猪去氧胆酸的含量。结果 鉴别方法专属性强;含量测定猪去氧胆酸在3.50~12.25μg内积分值与点样量呈线性,回收率为100.5%,RSD为3.2%。结论 本质量标准可用于肠安口服液的质量控制。

关 键 词:肠安口服液 猪胆汁 猪去氧胆酸 质量标准
修稿时间:1999-10-13

Study on the Quality Standard of Changan Oral Solution
S Wan,J Shan,X Zhang. Study on the Quality Standard of Changan Oral Solution[J]. Journal of Chinese medicinal materials, 2000, 23(1): 43-44
Authors:S Wan  J Shan  X Zhang
Affiliation:Kaifeng Medical College, 475001.
Abstract:OBJECTIVE: To study the quality standard of Changan oral solution. METHOD: Thin layer chromatography was used for identification pig's bile plaster. TLC scanning was used for the determination of hyodeoxycholic acid. RESULTS: The TLC identification was highly specific and the spots was clear and concentrated. Linear regression for hyodeoxycholic acid was over the range of 3.50-12.25 micrograms. The average recovery of hyodeoxycholic acid was 100.5%, RSD was 3.2%. CONCLUSION: This standard was capable to effectively control the quality of Changan oral solution.
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