| 检测壮腰补肾丸中非法掺入的枸橼酸西地那非 |
| |
| 引用本文： | 江生,张小松,杨必勇.检测壮腰补肾丸中非法掺入的枸橼酸西地那非[J].华西药学杂志,2006,21(6):590-592. |
| |
| 作者姓名： | 江生 张小松 杨必勇 |
| |
| 作者单位： | 重庆市药品检验所,重庆,401221;重庆市药品检验所,重庆,401221;重庆市药品检验所,重庆,401221 |
| |
| 摘 要： | 目的建立检查壮腰补肾丸中非法掺入枸橼酸西地那非的方法。方法采用薄层色谱、高效液相色谱(二极管阵列检测)和质谱分析方法检查。结果样品中检出了枸橼酸西地那非。结论所用方法专属性强、灵敏度高、操作简便,可作为药检部门监督打假的参考方法。
|
| 关 键 词： | 壮腰补肾丸 枸橼酸西地那非 薄层色谱 高效液相色谱 质谱 |
| 文章编号： | 1006-0103(2006)06-0590-03 |
| 收稿时间： | 2005-12 |
| 修稿时间： | 2005年12月1日 |
Determination of Sildenafile citrate mixed illegally in Zhuangyao Bushen pill |
| |
| JIANG Sheng,ZHANG Xiao-song,YANG Bi-yong.Determination of Sildenafile citrate mixed illegally in Zhuangyao Bushen pill[J].West China Journal of Pharmaceutical Sciences,2006,21(6):590-592. |
| |
| Authors: | JIANG Sheng ZHANG Xiao-song YANG Bi-yong |
| |
| Institution: | Chongqing Institute for Drug Control, Chongqing 401221, China |
| |
| Abstract: | OBJECTIVE To identify Sildenafile citrate mixed illegally in Zhuangyao Bushen pill.METHODS TLC and HPLC methods were established for the separation and determination of the organic solvent extract of the sample,and Sildenafile citrate was identified by DAD detector and MS.RESULTS Illegally mixed Sildenafile citrate in the sample was verified.CONCLUSION This method is accurate,simple and sensitive,and it can be used to detect Zhuangyao Bushen pill. |
| |
| Keywords: | Zhuangyao Bushen pill Sildenafile citrate TLC HPLC MS |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
