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妇科调经片中阿魏酸的含量测定
引用本文:冯素香,李明丽,王淑美.妇科调经片中阿魏酸的含量测定[J].河南中医药学刊,2008(5):39-40.
作者姓名:冯素香  李明丽  王淑美
作者单位:河南中医学院,河南郑州450008
摘    要:目的:建立妇科调经片中阿魏酸的含量测定方法。方法:采用大连依利特Betasil C18色谱柱(4.6×200mm,5μm);甲醇-0.1%磷酸溶液(30:70)为流动相;流速1.0ml/min,检测波长320nm,对当归和川芎中阿魏酸进行含量测定。结果:平均回收率为98.2%,RSD=0.88%。结论:该法简便、准确、专属性强,可作为妇科调经片的质量控制方法。

关 键 词:妇科调经片  阿魏酸  高效液相色谱  含量测定

DeterminAtion of Ferulic Acid in Fuketiaojing Tablet
Feng Suxiang,Li Mingli,Wang Shumei.DeterminAtion of Ferulic Acid in Fuketiaojing Tablet[J].Journal of Henan college of Traditional Chinese Medicine,2008(5):39-40.
Authors:Feng Suxiang  Li Mingli  Wang Shumei
Institution:( Henan College of Chinese Medicine, Zhengzhou, Henan, China, 450008)
Abstract:Object: To determine the content of ferulic acid in Fuketiaojing Tablet. Methods: The content of ferulic acid of Radix Angelicae Sinensis and Rhizoma Chuangxiong was determined by HPLC, and Using Betasil C18 column(4.6×200mm,5μm) , the mobile phase was a mixture of Methanol -0.1% phosphoric acid solution (30:70), the flow rate was 1.0ml/min, the wavelength was 320nm. Result: The average recovery was 98.2 %, RSD=0.88%. Conclusion: The method is simple, accurate, and can be used to control the effective parts quality.
Keywords:Fuketiaojing Tablet  ferulic acid  HPLC  determination of content
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