| 一测多评法测定假马齿苋中间体中的5种三萜皂苷类成分含量 |
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| 引用本文： | 崔雨晴,张继全,吴飞,阮克锋.一测多评法测定假马齿苋中间体中的5种三萜皂苷类成分含量[J].上海中医药杂志,2016,50(7):88-93. |
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| 作者姓名： | 崔雨晴 张继全 吴飞 阮克锋 |
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| 作者单位： | 上海中医药大学中药现代制剂技术教育部工程研究中心,上海,201203;上海张江中药现代制剂技术工程研究中心,上海,201203,上海中医药大学中药现代制剂技术教育部工程研究中心,上海,201203;上海张江中药现代制剂技术工程研究中心,上海,201203,上海中医药大学中药现代制剂技术教育部工程研究中心,上海,201203;上海张江中药现代制剂技术工程研究中心,上海,201203;上海中医药大学中药学院,上海,201203,上海中医药大学中药现代制剂技术教育部工程研究中心,上海,201203;上海张江中药现代制剂技术工程研究中心,上海,201203 |
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| 基金项目： | 上海市科委资助项目(15DZ2292000)；上海市科委科技支撑项目(15401902100) |
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| 摘 要： | 目的：利用一测多评法建立假马齿苋中间体中5种三萜皂苷类成分的高效液相色谱分析方法。 方法：以BacopasideⅠ为内参物,建立Bacoside A3、BacopasideⅡ、Bacopasaponin C isomer、Bacopasaponin C的相对校正因子,从而计算各成分含量,并将一测多评结果与外标法实测值用相对误差评价,验证一测多评法的准确性。 结果：BacopasideⅠ与Bacoside A3、BacopasideⅡ、Bacopasaponin C isomer、Bacopasaponin C的相对校正因子分别为0.980、0.747、1.046、0.836,一测多评法计算结果与外标法无显著差异,相对误差小于5%。 结论：该方法准确可靠,简便可行,可作为假马齿苋中间体多指标成分测定质量控制方法。
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| 关 键 词： | 假马齿苋 一测多评法 相对校正因子 外标法 假马齿苋皂苷Ⅰ 苦艾素A3 假马齿苋皂苷Ⅱ 假马齿苋皂苷C异构体 假马齿苋皂苷C |
| 收稿时间： | 2016/3/14 0:00:00 |
Simultaneous determination of five triterpenoid saponins in Bacopa monnieri extract by quantitative analysis of multi-components with a single marker |
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| CUI Yu-qing,ZHANG Ji-quan,WU Fei and RUAN Ke-feng.Simultaneous determination of five triterpenoid saponins in Bacopa monnieri extract by quantitative analysis of multi-components with a single marker[J].Shanghai Journal of Traditional Chinese Medicine,2016,50(7):88-93. |
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| Authors: | CUI Yu-qing ZHANG Ji-quan WU Fei and RUAN Ke-feng |
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| Institution: | Engineering Research Center of Modern Preparation Technology of Traditional Chinese Medicine, Ministry of Education, Shanghai University of Traditional Chinese Medicine, Shanghai, 201203;Engineering Research Center of Modern Preparation Technology of Traditional Chinese Medicine of Zhangjiang, Shanghai, 201203,Engineering Research Center of Modern Preparation Technology of Traditional Chinese Medicine, Ministry of Education, Shanghai University of Traditional Chinese Medicine, Shanghai, 201203;Engineering Research Center of Modern Preparation Technology of Traditional Chinese Medicine of Zhangjiang, Shanghai, 201203,Engineering Research Center of Modern Preparation Technology of Traditional Chinese Medicine, Ministry of Education, Shanghai University of Traditional Chinese Medicine, Shanghai, 201203;Engineering Research Center of Modern Preparation Technology of Traditional Chinese Medicine of Zhangjiang, Shanghai, 201203;College of Chinese Material Medica, Shanghai University of Traditional Chinese Medicine, Shanghai, 201203 and Engineering Research Center of Modern Preparation Technology of Traditional Chinese Medicine, Ministry of Education, Shanghai University of Traditional Chinese Medicine, Shanghai, 201203;Engineering Research Center of Modern Preparation Technology of Traditional Chinese Medicine of Zhangjiang, Shanghai, 201203 |
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