| 小儿清热止咳合剂的质量标准研究 |
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| 引用本文： | 王艳平,田杰,张宁惠. 小儿清热止咳合剂的质量标准研究[J]. 中国药房, 2006, 17(2): 138-139 |
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| 作者姓名： | 王艳平 田杰 张宁惠 |
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| 作者单位： | 宁夏自治区中医研究院,银川市,750021 |
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| 摘 要： | 目的:建立小儿清热止咳合剂的质量标准。方法:采用薄层色谱法对小儿清热止咳合剂中的麻黄、黄芩、甘草进行定性鉴别,以高效液相色谱法对其主要药材杏仁中的苦杏仁苷进行含量测定。结果:小儿清热止咳合剂中麻黄、黄芩、甘草的供试品薄层色谱中,在与对照品色谱相应的位置上,显相同颜色的斑点;苦杏仁苷进样量在0.198μg～4.954μg范围内与峰面积积分值线性关系良好(r=1.0000)。结论:本方法简便、准确、灵敏、重现性好,可用于本品的质量控制。
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| 关 键 词： | 小儿清热止咳合剂 薄层色谱法 苦杏仁苷 高效液相色谱法 质量标准 |
| 文章编号： | 1001-0408(2006)02-0138-02 |
| 收稿时间： | 2005-02-13 |
| 修稿时间： | 2005-07-11 |
Study on Quality Criteria of Fever and Cough Syrup for Children |
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| WANG Yanping,TIAN Jie,ZHANG Ninghui. Study on Quality Criteria of Fever and Cough Syrup for Children[J]. China Pharmacy, 2006, 17(2): 138-139 |
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| Authors: | WANG Yanping TIAN Jie ZHANG Ninghui |
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| Affiliation: | Research Institute of Chinese Traditional Medicine of Ningxia Autonomous Region, Yinchuan 750021, China |
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| Abstract: | OBJECTIVE:To establish the quality criteria of fever and cough syrup for children.METHODS:Thin-layer chromatography(TLC) was employed to make qualitative determination of herbba ephedrae,radix scutellariae,radix glycyrrhi-zae in fever and cough syrup for children,and high performance liquid chromatography(HPLC) was used to determine the con-tent of amygdaloside in its chief medicinal material,almond.RESULTS:The spots in the TLC of herbba ephedrae,radix scute-llariae,radix glycyrrhizae were in the same color with those in the chromatograms of control articles.The linear range of amygdaloside was 0.198μg～4.954μg(r=1.0 000).CONCLUSION:The present method is simple,accurate sensitiveness and highly reproductive,which can be used for the quality control of this preparation. |
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| Keywords: | Fever and cough syrup for children TLC Amygdalosidc HPLC Quality criteria |
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