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流苏石斛化学成分的研究(Ⅰ)
引用本文:毕志明,杨毅生,王峥涛,龚燕晴,何菊秀,豀忠人.流苏石斛化学成分的研究(Ⅰ)[J].中国药科大学学报,2001,32(3):42-44.
作者姓名:毕志明  杨毅生  王峥涛  龚燕晴  何菊秀  豀忠人
作者单位:1. 中国药科大学生药学研究室
2. 日本富山医科药科大学和汉药研究所
3. 日本富山医科药科大学和汉药研究所日本
摘    要:目的:从兰科植物流苏石斛(Denddrobium fimbriatum Hook.)茎中提取分离活性成分。方法:95%乙醇提取、溶剂抽提、硅胶柱层析、重结晶等。结果:分离出9个化合物,鉴定出其中6个,分别为大黄酚(3)、三十二烷酸(5)、对羟基反式肉桂酸三十烷基酯(6)、对羟基顺式肉桂酸三十烷基酯(7)、β-谷甾醇(8)和鼓槌联苄(9),结论:大黄酚为资产从石斛属植物中分得,鼓槌联苄为首次从该积木教授中分离得到。

关 键 词:流苏石斛  化学成分  大黄酚  鼓槌联苄  提取  分离
文章编号:1000-5048(2001)03-0200-03
修稿时间:2001年2月15日

Chemical Constituents of Dendrobium fimbriatum Hook.(
BI Zhi-ming,YANG Yi-Sheng,WANG Zheng-Tao,GONG Yan-Qing,HE Ju-Xiu,Tadato Tani.Chemical Constituents of Dendrobium fimbriatum Hook.([J].Journal of China Pharmaceutical University,2001,32(3):42-44.
Authors:BI Zhi-ming  YANG Yi-Sheng  WANG Zheng-Tao  GONG Yan-Qing  HE Ju-Xiu  Tadato Tani
Institution:BI Zhi Ming,YANG Yi Sheng,WANG Zheng Tao,GONG Yan Qing,HE Ju Xiu 1,Tadato Tani 1 Department of Pharmacognosy,China Pharmaceutical University,Nanjing 210038, 1Toyama Medical and Pharmaceutical University 2630 Sugitani,Toyama 930 0194,Ja
Abstract:AIM Bio-active constituents were expected to be obtained from Dendrobium fimbriatum Hook. METHODS It was extracted with 95% alcohol, distributed by petrol, isolated via column chromatography on silica gel and purified by crystallization. RESULTS Nine compounds were isolated from the stems of Dendrobium fimbriatum Hook., On the basis of spectral analyses, six compounds of them were identified as chrysophanol(3), n-dotriacodtanoic acid(5), defuscin(6), n-triacontyl cis-p-coumarate(7), β-sitosterol(8) and chrysotobibenzyl(9). CONCLUSION Chrysophanol(3) was firstly isolated from Genus dendrobium and chrysotobibenzyl(9) was found from this species for the first time.
Keywords:Dendrobium fimbriatum\  Chemical constituents  Chrysophanol  Chrysotobibenzyl
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