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HPLC法测定安肾丸中苦杏仁苷含量
引用本文:王敏,马玉梅. HPLC法测定安肾丸中苦杏仁苷含量[J]. 广州医药, 2012, 43(6): 32-33
作者姓名:王敏  马玉梅
作者单位:王敏 (贵州省安顺职业技术学院应用医药系 安顺561000) ; 马玉梅 (广东省深圳市泰康制药有限公司 518110) ;
摘    要:目的为了更好地控制安肾丸质量,对安肾丸中苦杏仁苷的含量进行测定。方法采用高效液相色谱法(HPLC)测定安肾丸中苦杏仁苷的含量。结果苦杏仁苷在10.25~512.5μg范围内线性关系良好,r=0.9999,平均回收率98.91%,RSD=0.48%。结论实验方法专属性强、重复性好,准确简便,可有效地控制安肾丸的质量。

关 键 词:安肾丸  高效液相色谱法  苦杏仁苷

Determination of amygdalin in Anshen Wan by HPLC
Wang Min,Ma Yumei. Determination of amygdalin in Anshen Wan by HPLC[J]. Guangzhou Medical Journal, 2012, 43(6): 32-33
Authors:Wang Min  Ma Yumei
Affiliation:1 Application of Chinese Medicine Department of Anshun Occupational Technology,Guizhou,Anshun 561000,China.2 Shenzhen Taikang Pharmacy Co.,Ltd.,Shenzhen 518110,China
Abstract:Objective To establish a method for the determination of effective components in Anshen Wan. Methods The contents of Amygdalin in Anshen Wan were dermined by HPLC. Results The resolutions of the dermined peaks of Amygdalin were fine at the lineatity range of 10.25~512.5μg. The average recoveries were 98. 91% with RSD 0. 48%, for Amygdalin respectively. Conclusion The experimental method is simple, accurate and good in stability specificity and repeatability, and can control the quality of this Anshen Wan.
Keywords:Anshen Wan  HPLC  Amygdalin
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