| 肉桂子药材的薄层鉴别方法研究 |
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| 引用本文： | 胡曙晨,马雪红,李新霞,李莉,热娜·卡斯木,支玲.肉桂子药材的薄层鉴别方法研究[J].西北药学杂志,2014(2):111-114. |
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| 作者姓名： | 胡曙晨 马雪红 李新霞 李莉 热娜·卡斯木 支玲 |
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| 作者单位： | 新疆医科大学药学院,乌鲁木齐830011 |
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| 基金项目： | 新疆维吾尔自治区科技重大专项 |
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| 摘 要： | 目的建立肉桂子药材的薄层鉴别系统。方法以桂皮醛和β-谷甾醇为对照品,对维药肉桂子进行薄层鉴别,并考察不同展开系统、不同点样量、不同薄层板、不同检视方式、不同温度和不同湿度对肉桂子药材薄层色谱的影响。结果以桂皮醛和β-谷甾醇为对照品,正己烷–乙酸乙酯(6∶1)为展开系统,肉桂子药材薄层鉴别特征明显,专属性强。结论该薄层方法可行,重复性好,可作为肉桂子药材的薄层鉴别方法。
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| 关 键 词： | 肉桂 桂皮醛 β-谷甾醇 薄层鉴别 |
Study on thin-layer chromatography identification methods for Fructus cinnamomi cassiae immaturi |
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| HU Shuchen,MA Xuehong,LI Xinxia,LI Li,Rena KASIM,ZHI Ling.Study on thin-layer chromatography identification methods for Fructus cinnamomi cassiae immaturi[J].Northwest Pharmaceutical Journal,2014(2):111-114. |
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| Authors: | HU Shuchen MA Xuehong LI Xinxia LI Li Rena KASIM ZHI Ling |
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| Institution: | (College of Pharmacy Xinjiang Medical University, Urumqi 830011, China) |
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| Abstract: | Objective To establish a thin-layer chromatography（TLC） identification method for the Uygur medicine Fructus cinnam-omi cassiae immaturi .Methods With cinnamic aldehyde and β-sitosterol as the references substances ,the TLC conditions ,such as the development system ,spotting sample volume ,thin layer chromatography plate ,inspection ,temperature and humidity ,were investigated .Results With cinnamic aldehyde andβ-sitosterol as the reference substances ,TLC identification for Fructus cinnam-omi cassiae immaturi was high specific with cyclohexane-ethyl acetate（6∶1） as the deployment system .Conclusion The estab-lished method is feasible and reproducible and could be used as the Fructus cinnamomi cassiae immaturi identification . |
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| Keywords: | Cinnamomum cassia Presl cinnamic aldehyde β-sitosterol TLC identification |
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