| 活血止痛散的制备与质量控制 |
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| 引用本文： | 张健萍,刘培.活血止痛散的制备与质量控制[J].中国药房,2005,16(13):992-993. |
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| 作者姓名： | 张健萍 刘培 |
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| 作者单位： | 1. 郑州市骨科医院,郑州市,450052
2. 河南中医学院,郑州市,450008 |
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| 摘 要： | 目的:制备活血止痛散并建立其质量控制方法。方法:采用薄层色谱法对活血止痛散中三七、乳香、血竭进行定性鉴别;采用薄层扫描法测定血竭中血竭素的含量。结果:血竭素高氯酸盐进样量在0.6μg～3.2μg范围内线性关系良好(r=0.9999),平均加样回收率为98.22%(RSD=1.53%)。结论:该制剂制备方法可行,质量控制方法简单、准确、重现性好。
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| 关 键 词： | 活血止痛散 三七 乳香 血竭 血竭素高氯酸盐 制备 质量控制 |
| 文章编号： | 1001-0408(2005)13-0992-02 |
| 修稿时间： | 2005年4月1日 |
Preparation and Quality Control of Powder of Promoting Blood Circulation to Arrest Pain |
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| ZHANG Jianping,LIU Pei.Preparation and Quality Control of Powder of Promoting Blood Circulation to Arrest Pain[J].China Pharmacy,2005,16(13):992-993. |
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| Authors: | ZHANG Jianping LIU Pei |
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| Abstract: | OBJECTIVE:To prepare powder of promoting blood circulation to arrest pain and to establish its quality conˉtrol method.METHODS:Qualitative identification of panax pseudo-ginseng,frankincense and dragon blood in the powder of promoting blood circulation to arrest pain was performed by TLC method.The content of dracorhodin in the dragon blood was determined by TLC Scanning Method.RESULTS:Good linear relationship was achieved when the sample size of dracorhodin perchlorate remained within the scope of0.6μg～3.2μg(r=0.9999).The average recovery rate was98.22%(RSD=1.53%).CONCLUSION:This preparation method is feasible,and the quality control method is simple,accurate and reproducible. |
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| Keywords: | Powder of promoting blood circulation to arrest pain Panax pseudo-g nseng Frankincense Dragon blood Dracorhodin perchlorate Preparation Quality control |
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