| 关东丁香化学成分的分离与鉴定 |
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| 引用本文： | 冯雪松,许 磊,高慧媛,吴立军.关东丁香化学成分的分离与鉴定[J].沈阳药科大学学报,2009,26(9):697-700. |
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| 作者姓名： | 冯雪松 许 磊 高慧媛 吴立军 |
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| 作者单位： | 1．沈阳药科大学 中药学院，辽宁 沈阳 110016；2．中国医科大学 药学院，辽宁 沈阳 110001 |
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| 摘 要： | 目的扩大关东丁香(Syringa veutina Kom)的药用资源。方法采用硅胶柱色谱等方法进行分离纯化,根据理化性质和波谱数据进行结构鉴定。结果分离得到6个化合物,分别鉴定为(-)-橄榄脂素((-)-olivil,1)、(-)-开环异落叶松脂素9-O-β-D-吡喃葡萄糖苷((-)-secoisrariciresinol-9-O-β-D-glucopyranoside,2)、橄榄苦苷(oleuropein,3)、demethyloleuropein(4)、10-羟基橄榄苦苷(10-hydroxyoleuropein,5)、lucidumoside C(6)。结论化合物2、6为丁香属植物中首次分离得到,化合物1、4、5为关东丁香植物中首次分离得到。
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| 关 键 词： | 关东丁香 化学成分 结构鉴定 |
| 收稿时间： | 2008-11-7 |
| 修稿时间： | 2008-12-7 |
Isolation and identification of chemical constituents of Syringa veutina Kom |
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| FENG Xue-song,XU Lei,GAO Hui-yuan,WU Li-jun.Isolation and identification of chemical constituents of Syringa veutina Kom[J].Journal of Shenyang Pharmaceutical University,2009,26(9):697-700. |
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| Authors: | FENG Xue-song XU Lei GAO Hui-yuan WU Li-jun |
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| Institution: | 1.School of Traditional Chinese Materia Medica, Shenyang Pharmaceutical University, Shenyang 110016, China；2.School of Pharmaceutical Science, China Medical University, Shenyang 110001,China |
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| Abstract: | Objective To study the chemical constituents of leaves of Syringa veutina Kom. Methods The compounds were isolated by chromatography on silica gel column and identified by the physico-chemical properties and spectral analysis. Results Six compounds were obtained and identified as （-）-olivil（1）, （-）-secoisrariciresinol-9-O-β-D-glucopyranoside（2）, oleuropein（3）, demethyloleuropein（4）, 10-hydroxyoleuropein（5）and lucidumoside C（6）.Conclusions Compound 2 and 6 are firstly isolated from genus syringa. Compounds 1,4 and 5 are isolated from this plant for the first time. |
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| Keywords: | Syringa veutina Kom chemical constituent structure identification |
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