| HPLC法测定驱风口服液中大黄素的含量 |
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| 引用本文： | 尹银华,周洪波.HPLC法测定驱风口服液中大黄素的含量[J].亚太传统医药,2010,6(1):31-32. |
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| 作者姓名： | 尹银华 周洪波 |
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| 作者单位： | 1. 遵义医学院第五附属,珠海,医院,广东珠海519100
2. 广东药学院中山校区,广东中山,528400 |
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| 摘 要： | 目的:建立驱风口服液中大黄素的含量测定方法。方法:采用高效液相色谱法,色谱柱:UtimateXB-C18(150mm×4.6mm,5μm);流动相:甲醇—0.1%磷酸溶液(80∶20);检测波长为254nm。结果:大黄素进样量在0.072～1.452μg的范围内与峰面积呈良好的线性关系(r=0.9996),平均回收率为103.2%,RSD为1.1%(n=6)。结论:本法简单、准确、重复性好,可以作为驱风口服液的质量控制方法。
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| 关 键 词： | HPLC 大黄素 驱风口服液 |
HPLC Determination of Emodin in Qufeng Oral Liquid |
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| Yin Yinhua,Zhou Hongbo.HPLC Determination of Emodin in Qufeng Oral Liquid[J].Asia-Pacific Traditional Medicine,2010,6(1):31-32. |
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| Authors: | Yin Yinhua Zhou Hongbo |
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| Institution: | 1.Fifth Affiliated Hospital of Zunyi Medical College ,Zhuhai 519100, China;2.Guangdong Pharmaceutical University Zhongshan campus,Zhongshan 528458 ,China) |
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| Abstract: | Objective：To establish an HPLC determination method for emodin in Qufeng Oral liquid.Methods：The Utimate XB-C18 （150mm×4.6mm,5μm） was used,the mobile phase consisted of methanol-0.1%phosphoric acid （80：20）,flow rate was 1mL.min-1 ,the detection wavelength was 254nm.Results：The linear range of emodin was 0.072 -1.452μg （r =0.9996）.The recovery of method was 103.2%, RSD was 1.1% （n =6）.onclusion ：The method is simple,accurate, repeatable. It is suitable for the routine quality control of Qufeng Oral liquid. |
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| Keywords: | HPLC Emdin Qufeng Oral Liguid |
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