首页 | 本学科首页   官方微博 | 高级检索  
检索        

萌生丸的质量标准
引用本文:黄德红,张勤.萌生丸的质量标准[J].中国药师,2010,13(6):815-816.
作者姓名:黄德红  张勤
作者单位:1. 襄樊市中医医院,湖北襄樊,441000
2. 襄樊市药品检验所
摘    要:目的:建立萌生丸的质量标准.方法:采用薄层色谱法对制剂中的当归、川芎、牡丹皮进行定性鉴别 采用高效液相色谱法对制剂中的阿魏酸进行含量测定.结果:在薄层色谱中能检出当归、川芎、牡丹皮等药材 阿魏酸的含量在0.041 2~0.329 6μg范围内与峰面积呈良好的线性关系(r=0.999 9),加样回收率为99.0%,RSD=0.80%(n=6).结论:该方法专属性强,灵敏度高,重复性好,操作简便,可有效控制萌生丸的质量.

关 键 词:萌生丸  阿魏酸  薄层色谱法  高效液相色谱法

Quality Standard for Mengsheng Pills
Huang Dehong,Zhang Qin.Quality Standard for Mengsheng Pills[J].China Pharmacist,2010,13(6):815-816.
Authors:Huang Dehong  Zhang Qin
Institution:(Xiangfan Institute for Drug Control)
Abstract:Objective: To establish the quality standard for mengsheng pills. Method: Radix angelicae sinensis, Rhizoma chuanxion, Contex moutan in mengsheng pills were identified by TLC,the content of paeonol was determined by HPLC. Result: The spots in the TLC were clear and distinguished well. the linear rang of paeonol was 0. 041 2-0. 329 6 μg,r =0. 999 9,the average recovery was 99. 0%, with RSD = 0. 8% ( n = 6). Conclusion: This method is simple and repeatable, it can be used for quality control of mengsheng pills.
Keywords:Mengsheng pills  Paeonol  TLC  HPLC
本文献已被 维普 万方数据 等数据库收录!
设为首页 | 免责声明 | 关于勤云 | 加入收藏

Copyright©北京勤云科技发展有限公司  京ICP备09084417号