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小柴胡冲剂质量标准的研究
引用本文:陈成刚,吴泽君. 小柴胡冲剂质量标准的研究[J]. 湖南中医药大学学报, 2000, 20(4): 20-22
作者姓名:陈成刚  吴泽君
作者单位:湖南省株洲市药品检验所,湖南,株洲412008
基金项目:湖南省珠洲市科技三项计划,49号,
摘    要:为制定小柴胡冲剂的质量标准,采用薄层层析法对小柴胡冲剂中的柴胡、甘草、黄芩进行了定性鉴别,用高效液相色谱法测定黄芩苷的含量。结果:柴胡、甘草、黄芩的生鉴别灵敏、专属;黄芩苷含量测定平均回收率100.5%,RSD=1.20%。结论:建立的定性、定量方法简便、准确、灵敏、重现性好,可作为其质量控制标准。

关 键 词:小柴胡冲剂 薄层色谱 高效液相色谱 质量标准

Studies on Quality Standards of Xiaochaihu Granule
Chen Chenggang,Wu Zejun. Studies on Quality Standards of Xiaochaihu Granule[J]. Journal of Traditional Chinese Medicine University of Hunan, 2000, 20(4): 20-22
Authors:Chen Chenggang  Wu Zejun
Abstract:OBJECTIVE:To work out the quality standards of Xiaochaihu Granules.METHODS:The identification of composition was carryied out with TLC.The determination of content of baicalin was performed with HPLC.RESULTS:The identification of Radix Bupleuri,Radix Glycyrrhizae and Radix scutellariae in Xiaochaihu Granules had been carryied out with TLC.The content of baicalin was determined by HPLC.The average recovery was 100.5%,with RSD 1.2%.CONCLUSION:The metheods of quantitative and qualitative analyses were simple,sensitive,accurate and with a good reproduction.These methods could be used to control the quality of Xiaochaihu Granules.
Keywords:Xiaochaihu granule  TLC  HPt  
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