| 石见穿化学成分研究 |
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| 引用本文： | 高俊峰,丁玲,张鹏,刘建勋.石见穿化学成分研究[J].中国中药杂志,2013,38(10):1556-1559. |
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| 作者姓名： | 高俊峰 丁玲 张鹏 刘建勋 |
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| 作者单位： | 中国中医科学院西苑医院实验研究中心,北京,100091 |
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| 基金项目： | 国家自然科学基金项目(81073060) |
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| 摘 要： | 该实验针对石见穿醋酸乙酯部位化学成分进行研究.采用硅胶、ODS、Sephadex LH-20柱色谱和高效液相制备色谱进行分离纯化,运用NMR和MS等波谱学方法,并结合文献对照确定了化合物的结构.从石见穿醋酸乙酯部位中分离鉴定了11个化合物,分别为:oresbiusin A(1),ethyl dihydrocaffeate (2),迷迭香酸乙酯(3),迷迭香酸(4),迷迭香酸甲酯(5),bis(2-ethylhexyl) phthalate(6),丹酚酸C(7),丹酚酸C甲酯(8),丹酚酸A甲酯(9),紫草酸B二甲酯(10),丹酚酸A(11).除迷迭香酸外,其他化合物均为首次从该植物中分离得到.
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| 关 键 词： | 石见穿 唇形科 化学成分 |
| 收稿时间： | 2013/2/24 0:00:00 |
Chemical constituents of Salvia chinensis |
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| GAO Jun-feng,DING Ling,ZHANG Peng and LIU Jian-xun.Chemical constituents of Salvia chinensis[J].China Journal of Chinese Materia Medica,2013,38(10):1556-1559. |
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| Authors: | GAO Jun-feng DING Ling ZHANG Peng and LIU Jian-xun |
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| Institution: | Research Center of Xiyuan Hospital, China Academy of Chinese Medical Sciences, Beijing 100091, China;Research Center of Xiyuan Hospital, China Academy of Chinese Medical Sciences, Beijing 100091, China;Research Center of Xiyuan Hospital, China Academy of Chinese Medical Sciences, Beijing 100091, China;Research Center of Xiyuan Hospital, China Academy of Chinese Medical Sciences, Beijing 100091, China |
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| Abstract: | Chemical constituents were investigated on the ethyl acetate extract of Salvia chinensis.Compounds were separated and purified by various chromatograhic techniques including silica gel,Sephadex LH-20 and reversed-phase HPLC. Their structures were identified by spectroscopic data analysis.Eleven compounds were isolated and purified and their structures were identified as oresbiusin A (1), ethyl dihydrocaffeate(2), ethyl rosmarinate(3), rosmarinic acid(4), methyl rosmarinate(5) , bis(2-ethylhexyl) phthalate (6), salvianol acid C(7), methyl salvianol acid C(8), methyl salvianolate A(9), dimethyl lithospermate B(10), and salvianolic acid A(11) .Except for rosmarinic acid, the remaining compounds were isolated from S. chinensis for the first time. |
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| Keywords: | Salvia chinensis Labiatae chemical constituents |
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