| GC法测定烧伤灵酊中右旋龙脑的含量 |
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| 引用本文： | 陈关键,陈爽.GC法测定烧伤灵酊中右旋龙脑的含量[J].中国药房,2011(31):2945-2946. |
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| 作者姓名： | 陈关键 陈爽 |
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| 作者单位： | 重庆市合川区中医院;重庆市疾病预防控制中心; |
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| 摘 要： | 目的:建立测定烧伤灵酊中右旋龙脑含量的方法。方法:采用气相色谱法。以水杨酸甲酯为内标物,采用氢火焰离子化检测器,分流进样,进样口温度为200℃,检测器温度为280℃,N(2载气)流速为45mL.min-1,H(2燃气)流速为40mL.min-1,空气(助燃气)流速为450mL.min-1。结果:右旋龙脑的检测浓度在0.2～0.7mg.mL-1范围内同其与内标的峰面积比值呈良好的线性关系(r=0.9998);平均加样回收率为98.75%,RSD=1.52%(n=9)。结论:本方法简便、灵敏、重复性好,可用于烧伤灵酊的质量控制。
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| 关 键 词： | 烧伤灵酊 气相色谱法 右旋龙脑 含量测定 |
Content Determination of D-borneol in Shaoshangling Tincture by GC |
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| CHEN Guan-jian CHEN Shuang.Content Determination of D-borneol in Shaoshangling Tincture by GC[J].China Pharmacy,2011(31):2945-2946. |
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| Authors: | CHEN Guan-jian CHEN Shuang |
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| Institution: | CHEN Guan-jian(Chongqing Hechuan District Hospital of TCM,Chongqing 401519,China) CHEN Shuang(Chongqing Center for Disease Prevention and Control,Chongqing 400042,China) |
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| Abstract: | OBJECTIVE：To establish the method for the content determination of D-borneol in Shaoshangling tincture.METHODS：GC method was adopted.FID detector was used with methyl salicylate as internal standard for sample injection;the injector temperature was 200℃ and the FID detector temperature was 280℃;the flow rates were 45 mL·min-1 for carrier gas（N2）,40 mL·min-1 for fuel gas（H2） and 450 mL·min-1 for assistant fuel gas（air）.RESULTS：The linear range of D-borneol was 0.2～0.7 mg·mL-1（r=0.999 8）with an average recovery of 98.75%（RSD=1.52%,n=9）.CONCLUSION：The method is simple,sensitive and reproducible.It can be used as the quality control for this preparation. |
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| Keywords: | Shaoshangling tincture GC D-borneol Content determination |
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