| 无梗五加果实化学成分的分离与鉴定 |
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| 引用本文： | 翟思佳,刘玉强,才谦.无梗五加果实化学成分的分离与鉴定[J].中华中医药学刊,2012(4):772-773. |
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| 作者姓名： | 翟思佳 刘玉强 才谦 |
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| 作者单位： | 辽宁中医药大学 |
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| 基金项目： | 辽宁省自然科学基金资助项目(20102147) |
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| 摘 要： | 目的:研究无梗五加Acanthopanax sessiliflorus(Ruqr.et Maxim)Seem.]果实的化学成分。方法:采用溶剂提取法、溶剂萃取法、硅胶柱层析法、凝胶柱层析法、重结晶法对无梗五加果实中的化合物进行分离纯化;根据光谱数据和理化性质确定化合物结构。结果:分离并鉴定了6个化合物,分别为:chiisanogenin(1),东莨菪内酯(2),胡萝卜苷棕榈酸酯(3),东莨菪苷(4),丁二酸(5),卫矛醇(6)。结论:化合物3、5、6为首次从无梗五加果实中分离得到。
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| 关 键 词： | 无梗五加 化学成分 结构鉴定 |
Isolation and Identification of Chemical Constituents from Fruits of Acanthopanax sessiliflorus(Ruqr.et Maxim)Seem. |
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| ZHAI Si-jia,LIU Yu-qiang,CAI Qian.Isolation and Identification of Chemical Constituents from Fruits of Acanthopanax sessiliflorus(Ruqr.et Maxim)Seem.[J].Chinese Archives of Traditional Chinese Medicine,2012(4):772-773. |
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| Authors: | ZHAI Si-jia LIU Yu-qiang CAI Qian |
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| Institution: | (Liaoning University of Traditional Chinese Medicine,Dalian 1l6600,Liaoning,China) |
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| Abstract: | Objective: To study the chemical constituents of the fruits of Acanthopanax sessiliflorus(Ruqr.et Maxim)Seem.Method:The methods of solvent extraction,silica gel column,Sephadex LH-20 column and recrystallizition were used for the isolation and spectroscopy methods were used for the structure identification.Results:6 compounds were isolated.They were identified as chiisanogenin(1),scopoletin(2),daucosterol palmitate(3),scopolin(4),succinate(5),galactitol(6).Conclusion:Compounds 3,5 and 6 were isolated from the fruits of Acanthopanax sessiliflorus(Ruqr.et Maxim)Seem.for the first time. |
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| Keywords: | Acanthopanax sessiliflorus chemical constituent structure identific ation |
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