| SPME-GC-MS联用分析大腹皮中挥发性成分 |
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| 引用本文： | 卢金清,李肖爽,梁欢,戴艺,张锐.SPME-GC-MS联用分析大腹皮中挥发性成分[J].北方药学,2012,0(10):8-9. |
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| 作者姓名： | 卢金清 李肖爽 梁欢 戴艺 张锐 |
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| 作者单位： | 湖北中医药大学/湖北省药用植物研发中心 |
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| 摘 要： | 目的:分析大腹皮中挥发性成分的化学组成。方法:采用顶空固相微萃取法(HS-SPME)萃取大腹皮中挥发性成分,并用气相色谱-质谱(GC-MS)联用技术对大腹皮的挥发性成分进行分析。结果:从大腹皮中共分离出60个色谱峰,鉴定出其中36种化合物,占总量的87.48%。其中主要成分为萘(54.93%)、二丁基羟基甲苯(7.21%)、3,4-二甲氧基甲苯(4.74%)等。结论:首次采用SPME-GC-MS联用技术分析大腹皮挥发性成分,为大腹皮的开发利用提供了科学依据。
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| 关 键 词： | 大腹皮 顶空-固相微萃取 气相色谱-质谱联用 挥发性成分 |
Analysis of the Volatile Constituents of Areca Pericarpium by SPME combined with GC-MS |
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| Lu Jinqing Li Xiaoshuang Liang Huan Dai Yi Zhang Rui.Analysis of the Volatile Constituents of Areca Pericarpium by SPME combined with GC-MS[J].BEIFANG YAOXUE,2012,0(10):8-9. |
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| Authors: | Lu Jinqing Li Xiaoshuang Liang Huan Dai Yi Zhang Rui |
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| Institution: | Lu Jinqing Li Xiaoshuang* Liang Huan Dai Yi Zhang Rui(Hubei University of Traditional Chinese Medicine/Medicinal Plant Research and Development Center of Hubei Province,Wuhan 430065,China) |
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| Abstract: | Objective:To analyze the compositions of volatile constitue- nts in Areca Pericarpium.Methods: The volatile constituents were extracted with headspace solid phase micro extraction(HS-SPME),and their contents and names were confirmed by GC-MS.Results: 60 compounds were identified from Areca Pericarpium and 36 of them were separated.The later made up 87.48% of the total amount.The main components obtained from Areca Pericarpium were Naphthalene(54.93%),Butylated Hydroxytoluene(7.21%) and 3,4-Dimethoxytoluene (4.74%).Conclusion: The compounds in Areca Pericarpium firstly confirmed in this study which will provide scientific evidence for the development of Areca Pericarpium. |
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| Keywords: | Areca Pericarpium HS-SPME GC-MS volatile components |
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