| HPLC测定补肾活血胶囊中异秦皮啶的含量 |
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| 引用本文： | 陈维静,齐海峰. HPLC测定补肾活血胶囊中异秦皮啶的含量[J]. 现代中药研究与实践, 2011, 0(3): 70-72 |
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| 作者姓名： | 陈维静 齐海峰 |
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| 作者单位： | [1]吉林通化振国药业有限公司,吉林通化134100 [2]辽宁九州龙跃药业有限公司,辽宁沈阳110016 |
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| 摘 要： | 目的 建立高效液相色谱法测定补肾活血胶囊中异秦皮啶的含量.方法 采用HPLC法测定制剂中异秦皮啶的含量.色谱柱:Kromasil TM C18柱(4.6 rn×150 mm,5μm);流动相:甲醇-水(30:70);流速:1 mL/min;检测波长:344nm.结果 异秦皮啶在0.020～0.200μg范围内线性良好(...
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| 关 键 词： | 高效液相色谱法 补肾活血胶囊 异秦皮啶 含量测定 |
Determination of Isofraxidin in Bu Shen Huo Xue Capsules by HPLC |
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| CHEN Wei-Jing,QI Hai-feng. Determination of Isofraxidin in Bu Shen Huo Xue Capsules by HPLC[J]. Research and Practice on Chinese Medicines, 2011, 0(3): 70-72 |
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| Authors: | CHEN Wei-Jing QI Hai-feng |
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| Affiliation: | 1. Jilin Tong Hua Zhen Guo Pharmaceutical Co.Ltd, Tonghua 134100,China; 2. Liaoning Jiu Zhou LongYue Pharmaceutical Co.Ltd, Shenyang 163319,China) |
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| Abstract: | Objective To establish an HPLC method for determination of isofraxidin in Bu Shen Huo Xue Capsules. Methods In this method Kromasil TM C18 column （4.6mm×150mm, 5μm） was used, methanolwater（30 ： 70） was used as a mobile phase .The detection wave-length was set at 344nm. Results The linear range were 0.020-0.200 μg （r=0.999 9）. The average recovery was 99.74% with RSD 0.42%. Conclusion This method is simple and the result is reliable. |
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| Keywords: | HPLC Bu Shen Huo Xue Capsules isofraxidin content determination |
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