| 氟的荧光测定法研究 |
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| 引用本文： | 李华斌 姚廷伸. 氟的荧光测定法研究[J]. 中国卫生检验杂志, 1994, 4(1): 3-5 |
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| 作者姓名： | 李华斌 姚廷伸 |
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| 作者单位： | 华西医科大学公共卫生学院，四川师范大学化学系 四川成都 610044 |
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| 摘 要： | 本文建立了氟的Al~(3 )—Calcein配合物荧光熄灭测定法。该法激发波长480nm,发射波长503nm,线性范围2—150ppbF~-,灵敏度为2ppbF~-,是现有的最灵敏方法之一。100ppbF~-时标准偏差为1.3ppbF~-。用茜素络合剂分光光度法进行对照试验,二者获得的结果一致。
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| 关 键 词： | 氟 荧光分析 |
Fluorometric Determination of Fluoride |
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| Li Huabin College of Public Health .West China University of Medical Sciences. Fluorometric Determination of Fluoride[J]. Chinses Journal of Health Laboratory Technology, 1994, 4(1): 3-5 |
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| Authors: | Li Huabin College of Public Health .West China University of Medical Sciences |
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| Affiliation: | Li Huabin College of Public Health .West China University of Medical Sciences (Chengdu 610044)Yao Tingshen Department of Chemistry .Sichuan Normal University(Chengdu 610066) |
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| Abstract: | This work was initiated in an effort to obtain a better method for the determination of trace fluoride. A fluoro -quenching method for the determination of fluoride with A13 - calcein complex is established. The excitation and emission wavelengths are 480nm and 503nm,with rectilinear range of 2 -150 ppb F-. The senstirity of the method is 2ppb F-and thestandard deviation 1. 3 ppb F-for 100ppb of fluoride. The results obtained agree with that by spectrophotometry with alizarin complexon. The accuracy and precision of the method is satisfactory. |
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| Keywords: | Fluoride Fluorometry |
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