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高效液相色谱法测定丹柴散结口服液中丹酚酸B的含量
引用本文:王伟丽,朱明伟,高芳. 高效液相色谱法测定丹柴散结口服液中丹酚酸B的含量[J]. 中国中医药现代远程教育, 2013, 11(5): 160-161
作者姓名:王伟丽  朱明伟  高芳
作者单位:王伟丽(河南省商丘市食品药品药检所,商丘,476000);朱明伟(河南省商丘市食品药品药检所,商丘,476000);高芳(河南省商丘市食品药品药检所,商丘,476000);
摘    要:目的建立丹柴散结口服液的质量标准。方法采用HPLC法对丹柴散结口服液中丹酚酸B的含量进行测定。结果丹柴散结口服液中丹酚酸B的含量在0.0081~0.1628μg的范围内,有良好的线性关系,r=0.9999,平均回收率为98.76%,RSD为1.04%。结论建立了丹柴散结口服液的质量标准,该方法操作易行,稳定可靠,用于丹柴散结口服液中丹酚酸B的含量,可以用于该制剂的质量控制。

关 键 词:丹柴散结口服液  丹酚酸B  HPLC

Determination of Paeoniflorin in Danchaisanjie Mixture by HPLC
Wang Weili,Zhu Mingwei,GaoFang. Determination of Paeoniflorin in Danchaisanjie Mixture by HPLC[J]. Chinese Medicine Modern Distance Education of China, 2013, 11(5): 160-161
Authors:Wang Weili  Zhu Mingwei  GaoFang
Affiliation:(Shangqiu Institute for Food and Drug Control , Shangqiu 476000 , China)
Abstract:Objective To establish a standard for determination of paeoniflorin in DanChaisanjie mixture. Method Paeoniflorin in DanChaisanjie mixture by HPLC. Result The linear range of paeoniflorin was 0. 0081-0. 1628μg , r = 0. 9999. The average recovery of paeoniflorin was 98. 76 %and RSD was 1.04 %. Conaosion The method is simple ,sensitive and aeeurte and can be used to determine paeoniflorin in DanChaisanjie mixture and quality control of DanChaisanjie mixture.
Keywords:DanChaisanjie mixturePaeoniflorinB  HPLC
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