| 洁阴灵洗液质量标准研究 |
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| 引用本文： | 黄俊,邓涛,侯富才,郭宗华.洁阴灵洗液质量标准研究[J].中国药业,2009,18(5):19-20. |
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| 作者姓名： | 黄俊 邓涛 侯富才 郭宗华 |
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| 作者单位： | 贵州神奇药物研究所,贵州,贵阳,550005 |
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| 摘 要： | 目的制订洁阴灵洗液的质量标准,方法用薄层色谱（TLC）法鉴别洁阴灵洗液中的苦参碱、龙脑及原药材蛇床子，用高效液相色谱（HPLC）法测定盐酸小檗碱的含量。结果盐酸小檗碱进样量在0．169～0．848μg范围内与峰面积线性关系良好，r=0．9995（n=5）；平均回收率为99．51％，RSD为2．33％（n=6）。结论所建立的方法能准确、快速地进行定性、定量检测，可用于洁阴灵洗液的质量控制。
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| 关 键 词： | 洁阴灵洗液 盐酸小檗碱 高效液相色谱法 薄层色谱 |
Study on Quality Standard for Jieyinling Lotion |
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| Huang Jun,Deng Tao,Hou Fucai,Guo Zonghua.Study on Quality Standard for Jieyinling Lotion[J].China Pharmaceuticals,2009,18(5):19-20. |
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| Authors: | Huang Jun Deng Tao Hou Fucai Guo Zonghua |
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| Institution: | (Guizhou Shenqi Drug Research Institute, Guiyang, Guizhou, China 550005) |
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| Abstract: | Objective To establish the quality control standard for Jieyinling Lotion. Methods Matrine, bomeol and Fructus Cnidii in Jieyinling Lotion were identified by TLC. The content of berberine hydroehloride was determined by RP-HPLC. Results Berberine hydrochlofide showed the good linear relationship at the range of 0. 169-0. 848 μg, r =0. 999 5（ n =5）. The average recovery rate was 99.51%, and RSD was 2.33% （n = 6）. Conclusion The method is accurate and quick. It can be used for the quality control of Jieyinling Lotion. |
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| Keywords: | Jieyinling Lotion berberine hydrochloride HPLC TLC |
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