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舒筋消痛胶囊质量标准的建立
引用本文:蒋云根,吴可柱,白玫.舒筋消痛胶囊质量标准的建立[J].武警医学院学报,2011,20(7):544-546,549.
作者姓名:蒋云根  吴可柱  白玫
作者单位:武警江西总队医院药剂科,江西南昌,330001
摘    要:【目的】建立舒筋消痛胶囊的质量控制标准。【方法】采用薄层色谱层析法对舒筋消痛胶囊的有效成分进行定性分析,然后通过高效液相色谱法对胶囊中续断的主要活性成分川续断皂苷Ⅵ进行含量测定。【结果】TCL鉴定方法专属性强;川续断皂苷Ⅵ在1.9688~19.688μg范围内线性关系良好,平均回收率为99.1%,RSD值为0.33%(n=5)。【结论】所建立的方法操作简单,结果准确,重复性好,可用于舒筋消痛胶囊的质量控制。

关 键 词:舒筋消痛胶囊  川续断皂苷Ⅵ  高效液相色谱  含量测定

Study on the quality standard of ShuJinXiaoTong capsules
JIANG Yun-gen,WU Ke-zhu,BAI Mei.Study on the quality standard of ShuJinXiaoTong capsules[J].Acta Academiae Medicinae CPAPF,2011,20(7):544-546,549.
Authors:JIANG Yun-gen  WU Ke-zhu  BAI Mei
Institution:JIANG Yun-gen,WU Ke-zhu,BAI Mei(Department of Pharmacy,Jiangxi Provincial Corps Hospital of Chinese People's Armed Police Force,Nanchang 330001,China)
Abstract:Objective] To establish the quality standard of ShuJinXiaoTong capsules. Methods] The active components of ShuJinXiaoTong capsules were determined by the TLC method, while HPLC was used for the determination of Asperosaponin Ⅵ in the sample. Results ] The TCL identification was highly specific and the spots were clear. The linear range of Asperosaponin Ⅵ was from 1.9688 - 19.688 μ g. The average recovery of Asperosaponin Ⅵ was 99.1% and RSD was 0.33% (n = 5). Conclusion] The constructed method was proved to be simple, accurate and had good repetitions, thus, it is reasonable that the content of the AsperosaponinⅥ can he used to establish the quality standard of ShuJinXiaoTong capsules.
Keywords:ShuJinXiaoTong capsules  Asperosaponin Ⅵ  HPLC  determination
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