| 气相色谱法测定少林正骨凝胶中樟脑、龙脑、薄荷脑的含量 |
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| 引用本文： | 张国民,杨工昶,齐赤虹,王海迪. 气相色谱法测定少林正骨凝胶中樟脑、龙脑、薄荷脑的含量[J]. 河南中医学院学报, 2009, 24(1) |
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| 作者姓名： | 张国民 杨工昶 齐赤虹 王海迪 |
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| 作者单位： | 张国民,Zhang Guomin(开封市食品药品检验所,河南,开封475002);杨工昶,齐赤虹,Yang Gongchang,Qi Chihong(河南省医药学校,河南,开封475001);王海,Wang Haidi(北海凯运药业有限公司,广西,北海536007) |
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| 摘 要： | 目的:建立气相色谱法测定少林正骨凝胶中樟脑、冰片、薄荷脑的含量测定.方法:色谱柱采用DB-5毛细管色谱柱30 m×0.25 mm(涂布厚度0.25μm);柱温为100℃.结果:樟脑对照品进样量在0.8μg～2.8μg范围内呈良好的线性关系(r=0.9999),平均回收率为98.83%,RSD为1.32%(n=6);龙脑对照品进样量在0.5μg～1.8μg范围内呈良好的线性关系(r=0.9999),平均回收率为99.17%,RSD=1.57%(n=6);薄荷脑进样量在0.5μg～1.7 μg范围内呈良好的线性关系(r=0.9999),平均回收率为99.49%,RSD为1.72%(n=6).结论:方法简便,可靠,准确,可用于该制荆的质量控制.
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| 关 键 词： | 少林正骨凝胶 樟脑 龙脑 薄荷脑 气相色谱法 |
Determination of camphor Borneolum Syntheicum Mentholum inShaolin Zhenggu Ning Jiao by GC |
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| Zhang Guomin,Yang Gongchang,Qi Chihong,Wang HaidiRegin Institute for Drug control,Kaifeng,Henan,China,Henan Pharmaceutical School,Beihai Kaiyun Pharmaceutical co.ltd.,Beihai,Guangxi. Determination of camphor Borneolum Syntheicum Mentholum inShaolin Zhenggu Ning Jiao by GC[J]. Journal of Henan University of Chinese Medicine, 2009, 24(1) |
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| Authors: | Zhang Guomin Yang Gongchang Qi Chihong Wang HaidiRegin Institute for Drug control Kaifeng Henan China Henan Pharmaceutical School Beihai Kaiyun Pharmaceutical co.ltd. Beihai Guangxi |
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| Affiliation: | Zhang Guomin1,Yang Gongchang2,Qi Chihong2,Wang Haidi3Regin Institute for Drug control,Kaifeng,Henan,China,475002Henan Pharmaceutical School,475001Beihai Kaiyun Pharmaceutical co.ltd.,Beihai,Guangxi,536007 |
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| Abstract: | |
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| Keywords: | Shaolin Zhenggu Ningjiao camphor Borneolum Syntheicum Mentholum GC |
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