| 薄层扫描法测定小儿胃疾宁合剂中黄芪甲苷的含量 |
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| 引用本文： | 代龙,周长征,刘文启. 薄层扫描法测定小儿胃疾宁合剂中黄芪甲苷的含量[J]. 中药新药与临床药理, 2001, 12(1): 41-42 |
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| 作者姓名： | 代龙 周长征 刘文启 |
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| 作者单位： | 1. 山东中医药大学，济南 250014
2. 临沂市中医院，山东临沂 276002 |
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| 摘 要： | 比较多种精制方法,优选薄层展开条件,采用氯仿-甲醇-水(63:35:10)10℃以下放置分层的下层液,于15-18℃展开,10%硫酸乙醇,105℃烘约3-5min显色,以λS=400nm,λR=700nm,薄层扫描测定黄芪甲苷含量.
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| 关 键 词： | 小儿胃疾宁合剂 黄芪甲苷 薄层色谱法 中药 |
| 文章编号： | 1003 -9783（2001）01-0041-02 |
| 修稿时间： | 1999-04-05 |
Determination of Astragaloside IV in Xiao'er Weijining Mixture b y TLC |
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| DAI Long,ZHOU Changzheng,Liu Wenqi. Determination of Astragaloside IV in Xiao'er Weijining Mixture b y TLC[J]. Traditional Chinese Drug Research & Clinical Pharmacology, 2001, 12(1): 41-42 |
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| Authors: | DAI Long ZHOU Changzheng Liu Wenqi |
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| Abstract: | To determine the content of astragaloside IV in Xiao' er Weijining Mixt ure, TCL conditions were optimized by comparing various refined methods. And the y were as follows: the underlayer of CHCl3-CH3OH-H2O(65∶35∶10) below 10 ℃was developed at 15～18℃ and sprayed with 10%H2SO4-C2H5OH,the heating tempe rature was 105℃ for 3～5 min,and λS=400 nm, λR =700 nm. |
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| Keywords: | @ Xiao'er Weijining mixture/analysis, a stragaloside IV/analysis TLC |
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