Effects of sterilization on the mechanical properties and the surface topography of nickel-titanium arch wires

The effects of sterilization on the mechanical properties and the surface topography were determined on 0.017 x 0.025-inch Nitinol and Titanal arch wires. Three approved heat sterilization methods were used: dry heat, formaldehyde-alcohol vapor, and steam autoclave. Elastic moduli were obtained on 1-inch segments in 3-point bending. Laser scans of flatwise wire surfaces were conducted to detect surface alterations--whether they were caused by tarnish, corrosion, or pitting. Tensile properties were determined on 7-inch lengths: the 0.1% yield strength, the ultimate tensile strength, and the percent elongation at break. Within the confines of the present sterilization experiments, no detrimental changes were observed for either the selected mechanical properties or the surface topography. When the mean values of the two products were compared, Nitinol was less compliant but stronger than Titanal. Laser spectroscopy showed that Titanal possessed at least three times more specular reflectivity than Nitinol.