| 正交试验法优选舒郁煎膏水提工艺 |
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| 引用本文： | 于佳,刘瑶,张建玲,王欣欣,贺祝英.正交试验法优选舒郁煎膏水提工艺[J].中国实验方剂学杂志,2012,18(8):31-33. |
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| 作者姓名： | 于佳 刘瑶 张建玲 王欣欣 贺祝英 |
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| 作者单位： | 贵阳中医学院第一附属医院,贵阳,550002 |
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| 基金项目： | 中医药、民族医药科学技术研究项目([2009]79) |
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| 摘 要： | 目的:优选舒郁煎膏的水提工艺.方法:以浸膏得率和栀子苷含量为评价指标.栀子苷含量采用高效液相色谱法测定,采用L9(3)4正交试验设计筛选舒郁煎膏的最佳水提工艺条件.结果:最佳水提工艺为加12倍量水,浸泡1h,煎煮3次,分别煎煮1.5,1,1h.结论:优选得到的水提工艺稳定可行,适合于工业化生产,为舒郁煎膏的制剂研究提供参考.
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| 关 键 词： | 舒郁煎膏 正交试验 浸膏得率 栀子苷 高效液相色谱法 |
| 收稿时间： | 2011/11/27 0:00:00 |
Optimization of Water Extraction Process of Shuyu Decoction by Orthogonal Test |
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| YU Ji,LIU Yao,ZHANG Jian-ling,WANG Xin-xin and HE Zhu-ying.Optimization of Water Extraction Process of Shuyu Decoction by Orthogonal Test[J].China Journal of Experimental Traditional Medical Formulae,2012,18(8):31-33. |
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| Authors: | YU Ji LIU Yao ZHANG Jian-ling WANG Xin-xin and HE Zhu-ying |
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| Institution: | First Affiliated Hospital, Guiyang College of Traditional Chinese Medicine, Guiyang 550002, China;First Affiliated Hospital, Guiyang College of Traditional Chinese Medicine, Guiyang 550002, China;First Affiliated Hospital, Guiyang College of Traditional Chinese Medicine, Guiyang 550002, China;First Affiliated Hospital, Guiyang College of Traditional Chinese Medicine, Guiyang 550002, China;First Affiliated Hospital, Guiyang College of Traditional Chinese Medicine, Guiyang 550002, China |
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| Abstract: | Objective: To optimize water extraction process of Shuyu decoction. Method: With extract yield of aqueous extract and the content of geniposide as indexes,the content of geniposide was determined by HPLC,optimum water extraction conditions was selected by L9(3)4orthogonal design. Result: Optimal water extraction process of Shuyu decoction was:12 times the amount of water, soaked 1 h, extracted 3 times with 1.5,1,1 h,respectively. Conclusion: Optimized water extraction process was stable,feasible and suited for industrial production.It could settle foundation for preparation study of Shuyu decoction. |
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| Keywords: | Shuyu decoction orthogonal test yield of extract geniposide HPLC |
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