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小飞蓬挥发性化学成分的GC-MS分析
引用本文:邵帅,严铭铭,毕胜男,万志强,周媛,闫向竹,孙永嘉.小飞蓬挥发性化学成分的GC-MS分析[J].中国实验方剂学杂志,2012,18(8):116-117.
作者姓名:邵帅  严铭铭  毕胜男  万志强  周媛  闫向竹  孙永嘉
作者单位:长春中医药大学,长春,130117
基金项目:国家重大新药创制专项(2009ZX09103-323)
摘    要:目的:用GC-MS分析小飞蓬挥发油的化学成分.方法:采用水蒸气蒸馏法提取小飞蓬挥发油,利用GC-MS对所提取的挥发油成分进行分离鉴定,并用色谱峰面积归一化法计算各成分的相对百分含量.结果:鉴定出小飞蓬挥发油成分中26个化合物,占所提取挥发油总量的98.25%.主要成分为:柠檬烯(58.30%)、2,6-二甲基-6-(4-甲基-3-戊烯基)二环3.1.1]-2-庚烯(8.7%)、β-蒎烯(6.28%)、2-甲基-6-(4-甲基苯基)-2-庚烯(5.13%)、棕榈酸(5.07%)、月桂烯(4.52%)、1,3,5-三亚甲基-环庚烷(2.05%).结论:小飞蓬挥发油主要成分为柠檬烯.

关 键 词:小飞蓬  挥发油  GC-MS
收稿时间:2011/12/15 0:00:00

Analysis of Constituents of Volatile Oil from Erigeron canadensis by GC-MS
SHAO Shuai,YAN Ming-ming,BI Sheng-nan,WAN Zhi-qiang,ZHOU Yuan,YAN Xiang-zhu and SUN Yong-jia.Analysis of Constituents of Volatile Oil from Erigeron canadensis by GC-MS[J].China Journal of Experimental Traditional Medical Formulae,2012,18(8):116-117.
Authors:SHAO Shuai  YAN Ming-ming  BI Sheng-nan  WAN Zhi-qiang  ZHOU Yuan  YAN Xiang-zhu and SUN Yong-jia
Institution:Changchun University of Traditional Chinese Medicine, Changchun 130117, China;Changchun University of Traditional Chinese Medicine, Changchun 130117, China;Changchun University of Traditional Chinese Medicine, Changchun 130117, China;Changchun University of Traditional Chinese Medicine, Changchun 130117, China;Changchun University of Traditional Chinese Medicine, Changchun 130117, China;Changchun University of Traditional Chinese Medicine, Changchun 130117, China;Changchun University of Traditional Chinese Medicine, Changchun 130117, China
Abstract:Objective:To analyze the constituents of volatile oil from Erigeron canadensis by GC-MS.Method: The volatile oil was extracted by steam distillation,and then separated by capillary gas chromatography.The constituents of volatile oil were identified and their amount was determined by normalization method.Result: Twenty-six components were identified from E.canadensis and their amount accounted 98.25% of total volatile oil.The main components were limonene(58.30%),2,6-dimethyl-6-(4-methyl-3-pentenyl) bicyclo -2-heptene(8.7%),β-pinene(6.28%),2-methyl-6-(4-methyl-phenyl)-2-heptene(5.13%),palmitic acid(5.07%),myrcene(4.52%),1,3,5-trimethylene-cycloheptane(2.05%).Conclusion: The main component of volatile oil from E.canadensis is limonene.
Keywords:Erigeron canadensis  volatile oil  GC-MS
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