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中药白及的化学成分研究(I)
引用本文:韩广轩 王立新 等. 中药白及的化学成分研究(I)[J]. 第二军医大学学报, 2002, 23(4): 443-445
作者姓名:韩广轩 王立新 等
作者单位:[1]解放军第534医院,洛阳471003 [2]深圳市药检所
摘    要:目的:研究中药白及的化学成分。方法:用多种层析方法分离甲醇提取物,根据理化性质和波谱分析鉴定化合物的结构。结果:分离并鉴定了5个化合物,分别是2,7-二羟基-4-甲氧基-9,10-二氢菲(2,7-dihydroxy-4-methoxy-9,10-dihydrophenanthrene)(1);2,7-二羟基-3,4二甲氧基菲(2,7-dihydroxy-3,4-dimethoxyphenanthrene)(2);3,7-二羟基-2,4-二甲氧基菲(3,7-dihydroxy-2,4-dimethoxyphenanthrene)(3);3‘,3-二羟基-5-甲氧基联苄(3‘,3-dihydroxy-5-methoxybibenzyl)(4);对羟基苯甲醛(p-hydroxybenzaldehyde)(5)。结论:化合物2,3,4是首次从兰科植物白及中分离得到的。

关 键 词:化学成分 理化性质 波谱分析 白及 中草药 药物分析

Study on chemical constituents of Bletilla striata(I)
HAN Guang-Xuan,WANG Li-Xin,ZHANG Wei-Dong,YANG Zhi,LI Ting-Zhao,JIANG Tao,LIU Wen-Yong. Study on chemical constituents of Bletilla striata(I)[J]. Former Academic Journal of Second Military Medical University, 2002, 23(4): 443-445
Authors:HAN Guang-Xuan  WANG Li-Xin  ZHANG Wei-Dong  YANG Zhi  LI Ting-Zhao  JIANG Tao  LIU Wen-Yong
Abstract:Objective: To study the chemical constituents of Bletilla striata (Thunb. ) Reichb. f. Methods: The con-stituents were separated and purified by column chromatography with silica gel and Sephadex LH-20,and were identified byspectral analysis. Results: Five compounds were identified as: 2, 7-dihydroxy-4-methoxy-9, 10-dihydrophenanthrene (1), 2, 7-dihydroxy-3, 4-dimethoxyphenanthrene (2), 3, 7-dihydroxy-2, 4-dimethoxyphenanthrene (3 ), 3', 3--dihydroxy--5-methoxybiben-zyl(4), p-hydroxybenzaldehyde (5), Conclusion: Compound 2, 3, 4 are isolated from this plant for the first time.
Keywords:Blettila stritata  drug analysis   herbal  phenanthrene  bibenzyl
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