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气相色谱法测定骨疽康膏中麝香酮的含量
引用本文:于红艳,董玉秀. 气相色谱法测定骨疽康膏中麝香酮的含量[J]. 河南中医学院学报, 2006, 21(2): 35-36
作者姓名:于红艳  董玉秀
作者单位:河南省中医院,河南郑州450008
摘    要:目的:以麝香酮含量为指标对骨疽康膏进行质量控制.方法:用气相色谱法测定骨疽康膏中麝香酮的含量.结果:麝香酮在0.3064~1.5320μg范围内线性关系良好(r=0.998);精密度试验,RSD=1.43%;稳定性试验,RSD=2.6%;加样回收率试验,RSD=4.18%;重复性试验,RSD=3.74%.结论:本法测定骨疽康膏中麝香酮含量专属、可行.

关 键 词:麝香酮  骨疽康膏  气相色谱法
文章编号:1672-6839(2006)02-0035-02
修稿时间:2005-12-05

Determination of Muscone in Gujukang Extract by Gas Chromatography
Yu Hongyan,Dong Yuxie. Determination of Muscone in Gujukang Extract by Gas Chromatography[J]. Journal of Henan University of Chinese Medicine, 2006, 21(2): 35-36
Authors:Yu Hongyan  Dong Yuxie
Abstract:Objective: To control the quality of Gujukang with the target of muscone content. Method: The muscone content in Gujukang Extract was determined by gas chromatography. Result: The muscone had a good linear relationship between the range from 0.3064 to 1.5320. The accuracy experiment had 1.43% of RSD. The stability test had2.69% of RSD. The recovery rate test of added sample had 4.18% of RSD. The duplicated experiment had 3.74% of RSD. Conclusion: Gas chromatography is exclusive and feasible in determining muscone content in Gujukang Extract.
Keywords:muscone  Gujukanggao  gas chromatography
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