| HS-SPME-GC-MS联用分析稳心颗粒中的挥发性成分 |
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| 引用本文： | 吴红华,王忠平,南国,陈应鹏,卢成淑,朱彦.HS-SPME-GC-MS联用分析稳心颗粒中的挥发性成分[J].中国实验方剂学杂志,2015,21(11):73-76. |
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| 作者姓名： | 吴红华 王忠平 南国 陈应鹏 卢成淑 朱彦 |
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| 作者单位： | 天津中医药大学 天津市现代中药重点实验室, 天津 300193;天津国际生物医药联合研究院 中药新药研发中心, 天津 300457,天津中医药大学 天津市现代中药重点实验室, 天津 300193;天津国际生物医药联合研究院 中药新药研发中心, 天津 300457,天津中医药大学 天津市现代中药重点实验室, 天津 300193;天津国际生物医药联合研究院 中药新药研发中心, 天津 300457,天津中医药大学 天津市现代中药重点实验室, 天津 300193;天津国际生物医药联合研究院 中药新药研发中心, 天津 300457,天津中医药大学 天津市现代中药重点实验室, 天津 300193;天津国际生物医药联合研究院 中药新药研发中心, 天津 300457,天津中医药大学 天津市现代中药重点实验室, 天津 300193;天津国际生物医药联合研究院 中药新药研发中心, 天津 300457 |
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| 基金项目： | 国家科技部国际合作项目(2013DFA31620) |
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| 摘 要： | 目的:对稳心颗粒进行挥发性成分的快速分析,明确其主成分及相对含量。方法:采用顶空固相微萃取(HSSPME)与气相色谱-质谱(GC-MS)联用技术对稳心颗粒中的挥发性成分进行提取及快速分析,检索NIST08.L质谱库(匹配度≥80%),并结合文献报道鉴定了其中的化学成分。结果:从稳心颗粒挥发性成分中共鉴定出52种化合物,占总挥发性成分的67.39%,其中匙叶桉油烯醇、异丁香烯、氧化丁香烯、香橙烯等8个化合物为其主要成分,与文献报道的甘松挥发油主成分基本一致。结论:通过对其挥发性成分进行分析,为进一步研究稳心颗粒的药效物质基础提供了科学依据,并为其质量控制研究打下实验基础。
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| 关 键 词： | 稳心颗粒 顶空固相微萃取 气相色谱质谱联用 挥发性成分 |
| 收稿时间： | 2014/9/16 0:00:00 |
Analysis of Volatile Components of Wenxin Granule by HS-SPME-GC-MS Technique |
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| WU Hong-hu,WANG Zhong-ping,NAN Guo,CHEN Ying-peng,LU Cheng-shu and ZHU Yan.Analysis of Volatile Components of Wenxin Granule by HS-SPME-GC-MS Technique[J].China Journal of Experimental Traditional Medical Formulae,2015,21(11):73-76. |
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| Authors: | WU Hong-hu WANG Zhong-ping NAN Guo CHEN Ying-peng LU Cheng-shu and ZHU Yan |
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| Institution: | Tianjin State Key Laboratory of Modern Chinese Medicine of Tianjin University of Traditional Chinese Medicine(TCM), Tianjin 300193, China;Research and Development Center of TCM of Tianjin International Joint Academy of Biotechnology and Medicine, Tianjin 300457, China,Tianjin State Key Laboratory of Modern Chinese Medicine of Tianjin University of Traditional Chinese Medicine(TCM), Tianjin 300193, China;Research and Development Center of TCM of Tianjin International Joint Academy of Biotechnology and Medicine, Tianjin 300457, China,Tianjin State Key Laboratory of Modern Chinese Medicine of Tianjin University of Traditional Chinese Medicine(TCM), Tianjin 300193, China;Research and Development Center of TCM of Tianjin International Joint Academy of Biotechnology and Medicine, Tianjin 300457, China,Tianjin State Key Laboratory of Modern Chinese Medicine of Tianjin University of Traditional Chinese Medicine(TCM), Tianjin 300193, China;Research and Development Center of TCM of Tianjin International Joint Academy of Biotechnology and Medicine, Tianjin 300457, China,Tianjin State Key Laboratory of Modern Chinese Medicine of Tianjin University of Traditional Chinese Medicine(TCM), Tianjin 300193, China;Research and Development Center of TCM of Tianjin International Joint Academy of Biotechnology and Medicine, Tianjin 300457, China and Tianjin State Key Laboratory of Modern Chinese Medicine of Tianjin University of Traditional Chinese Medicine(TCM), Tianjin 300193, China;Research and Development Center of TCM of Tianjin International Joint Academy of Biotechnology and Medicine, Tianjin 300457, China |
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| Abstract: | |
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| Keywords: | Wenxin granules HS-SPME GC-MS volatile oil |
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