| 宫宁颗粒质量标准研究 |
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| 引用本文： | 林嘉民,陈娴瑛,花仲卉.宫宁颗粒质量标准研究[J].中国药房,2006,17(20):1582-1583. |
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| 作者姓名： | 林嘉民 陈娴瑛 花仲卉 |
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| 作者单位： | 厦门中山医院药学部,厦门市,361004 |
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| 摘 要： | 目的:建立宫宁颗粒的质量标准。方法:采用薄层色谱法对宫宁颗粒中的黄芩苷进行定性鉴别;以高效液相色谱法测定黄芩苷的含量。结果:供试品薄层色谱中,在与黄芩苷对照品相应的位置上显相同颜色的斑点;黄芩苷检测浓度在20～100μg/ml范围内与峰面积积分值线性关系良好,平均回收率为99.71%(RSD=1.23%)。结论:所建质量标准可用于本品的质量控制。
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| 关 键 词： | 宫宁颗粒 薄层色谱法 高效液相色谱法 黄芩苷 质量标准 |
| 文章编号： | 1001-0408(2006)20-1582-02 |
| 收稿时间： | 05 20 2006 12:00AM |
| 修稿时间： | 06 20 2006 12:00AM |
Study on Quality Standard of Gongning Granule |
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| LIN Jiamin,CHEN Xianying,HUA Zhonghui.Study on Quality Standard of Gongning Granule[J].China Pharmacy,2006,17(20):1582-1583. |
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| Authors: | LIN Jiamin CHEN Xianying HUA Zhonghui |
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| Institution: | Dept. of Pharmacy, Xiamen Zhongshan Hospital, Xiamen 361004, China |
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| Abstract: | OBJECTIVE:To establish a quality standard for Gongning granule.METHODS:Baicalin was identified qualitatively by TLC and the content of which was determined by HPLC.RESULTS:In the TLC of the testing sample,the same color spots were noted at the corresponding sites of the reference substance of baicalin.The linear range of baicalin was 20～100μg/ml and the average recovery was 99.71%(RSD=1.23%).CONCLUSION:This method is fast,simple,accurate and reproducible,and suitable for the quality control of Gongning granule. |
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| Keywords: | Gongning granule TLC HPLC Baicalin Quality standard |
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